Novel Instrumentation for High-Speed AFM-based Nano Machining

Lead Research Organisation: CARDIFF UNIVERSITY
Department Name: Sch of Engineering

Abstract

The development of novel and disruptive nano-scale manufacturing technologies is a research area of high importance. Although vacuum and mask-based lithography techniques are already employed in industry for nano-scale manufacturing of semi-conductor devices and the derived nano electro mechanical systems (NEMS) components, they still have a number of limitations associated with them. In particular, these fabrication technologies rely on capital-intensive equipment while being restricted to the fabrication of planar features and constrained to a limited set of processed materials. Besides, there are also increased concerns over their environmental friendliness as they are energy and resource intensive and generate significant waste.

In this context, this proposal will focus on the development of high-speed AFM probe-based mechanical machining at nano scale. The process represents an alternative and innovative solution that can potentially address the lack of cost effective, 3 dimensional and more environmentally friendly fabrication technologies for producing nano-structured components in a wide range of materials. However, to fully realise the potential of AFM probe-based machining, a step-change in its throughput is still required. For this reason, the research put forward in this project aims to develop a new actuation device that could be readily fitted on commercial AFM instruments to reach untapped processing speeds when conducting tip-based machining operations.

This new actuation device, which will rely on piezo-electric actuators, will be fixed onto the stage of AFMs and will be used to create fast rotating displacements of a processed sample with respect to the tip of an AFM probe. The vision is to enhance the capability of current AFM systems by enabling them to perform nano-scale material removal operations at cutting speeds a thousand times faster compared to state of the art in this field. In particular, the developed set-up will be designed so that it enables cutting speeds from a few m/min up to a few hundreds of m/min to be reached.

Two major advantages are envisaged with the development of this new set-up. First, it will provide a cost-effective and environmentally friendly alternative to vacuum and mask-based lithography techniques for nano-scale fabrication. Second, due to the fact that AFMs are widespread in research laboratories, it will contribute to broaden the base of users with in-house manufacturing capabilities for the nano-machining of components with sub-micrometre structures.

Planned Impact

The project outcome could result in addressing a number of issues, which cannot be tackled simultaneously by the current vacuum and mask-based nano-manufacturing processes. In particular, the production of three dimensional nano-structures in a cost-effective manner and in a broad range of material continues to remain a major challenge despite the fact that such nano-structured components can readily find applications in emerging fields such as photonics, biosensors, fuel cells and data storage. Thus, from an economic point of view, the project will contribute to the creation of more accessible and more environmentally friendly capabilities for the production of nanotechnology-based devices. In turn, this should open the door to an increased number of small and medium size enterprises and more modest research labs to consider and benefit from nanotechnology-enabled solutions.

In the long-term, the wider society will also benefit from the proposed research programme. This should be achieved by enabling the development of novel nanotechnology-based products with potential applications for improving public health, well-being and security.
 
Description Through the research funded on this grant, it was discovered that a theoretical cutting speed just over 5 m/min at the interface between the tool and the workpiece could be achieved with the AFM tip-based nanomachining process by modifying a commercial AFM set-up with the help of piezoelectric actuation technology.
Exploitation Route Piezoelectric actuators and AFM instruments are relatively widespread in research laboratories. The findings may be used by others to implement AFM-based nano-machining at higher cutting speed that the current state-of-the-art.
Sectors Electronics,Manufacturing, including Industrial Biotechology

 
Description AFM-based nano-machining: developing and validating a novel modelling approach for effective process implementation in nanotechnology applications
Amount £692,656 (GBP)
Funding ID EP/T01489X/1 
Organisation Engineering and Physical Sciences Research Council (EPSRC) 
Sector Public
Country United Kingdom
Start 05/2020 
End 05/2023
 
Title AFM tip-based nanomachining with increased cutting speed at the tool-workpiece interface 
Description his is the complete dataset for a study which aimed to enhance the throughput of the Atomic Force Microscopy (AFM) tip-based nanomachining process by increasing the cutting speed at the interface between the tool and the workpiece. A modified AFM set-up was implemented, which combined the fast reciprocating motions of a piezoelectric actuator, on which a PMMA workpiece was mounted, and the linear displacement of the AFM stage, which defined the length of produced grooves. The dataset comprises a number of related data sub-set as follows: 1) Measured amplitude of a piezoelectric actuator (model NAC2402-H2.3, Noliac, Denmark) reciprocating motions as a function of the driving frequency for an input peak-to-peak voltage of 225 V. 2) Measured groove depth, height of the pile-up on both sides of a groove and groove width as a function of the frequency utilsed to machine the grooves. 3) AFM images of machined grooves with frequencies of 10 Hz, 10 kHz and 40 kHz for a stage velocity of 100 µm/s along the 'edge-forward' feed direction. 4) Profiles of the groove cross-sections shown with sub-set (3) above. 5) Scanning electron microscopy images of the grooves shown with sub-set (3) above. 6) Measured groove depth, height of the pile-up on both sides of a groove and groove width as a function of the frequency of the piezoelectric actuator and the feed direction. 7) AFM images of machined grooves with different feed directions for a stage velocity of 100 µm/s and a frequency of 10 kHz. 8) Profiles of the groove cross-sections shown with sub-set (7) above. 9) Scanning electron microscopy images of the grooves shown with sub-set (7) above. 10) Evolution of the voltage signals (both before and after filtering) along the vertical and horizontal axes of the Position Sensitive Photo Diode (PSPD) and stage displacement signal for different feed directions for a stage velocity of 100 µm/s and a frequency of 10 kHz. 11) Measured groove depth, height of pile-up on both sides of a groove and width as a function of the feed value utilised. 12) AFM images of machined grooves with different feed values for the 'edge-forward' configuration and a frequency of 10 kHz. 13) Profiles of the groove cross-sections shown with sub-set (12) above. 14) Scanning electron microscopy images of the grooves shown with sub-set (12) above. 
Type Of Material Database/Collection of data 
Year Produced 2018 
Provided To Others? Yes  
Impact Research results based upon these data are published at https://doi.org/10.1016/j.precisioneng.2017.10.009 
 
Title An approach for characterizing and modelling the non-linearity of piezoelectric actuators when operated with high electric field and high frequency signals 
Description The dataset comprises a number of related data sub-sets as follows: 1) Experimental data showing (a) the plot of displacements of a shear piezoelectric plate under different voltage and frequency values, (b) variations of displacement and phase lag versus logarithmic frequency under a voltage of +/-125 V and (c) three examples of typical displacement plots, again under the voltage of +/-125 V. 2) Experimental data and fitting based on the model from Mueller and Zhang (Journal of Applied Physics, 1998, 83 (7), 3754-3761) for varying values of the piezoelectric coefficient 15 with an electric field, 1, under different frequencies between 2 Hz and 2 kHz. 3) Experimental data and fitting based on the model from Damjanovic (Physical Review B, 1997, 55(2), R649-R652) to express (a) the low field piezoelectric constant lin() and (b) the nonlinear coefficient of piezoelectric constant nl(). 4) Data showing a) displacements of a piezoelectric actuator for peak-to-peak voltage values in the range 100 V to 640 V and for frequency values from 2 Hz to 2000 Hz and (b) the predicted 3-dimensional plot of such displacement as a function of driving frequency and voltage. 5) Simulated data showing (a) displacements of a single piezoelectric plate at two different driving voltage and three frequency values, (b) resultant displacements from two piezoelectric plates actuated with sinusoidal signals 90°out-of-phase, (c) simulated boundary conditions with different mechanical loads and (d) effect of different load types on piezoelectric displacement. 6) Data showing a) comparison between the measured width at the bottom of a machined groove and the predicted frequency-dependent variation of displacement under the voltage of +/-140 V, (b) SEM images of machined nanogrooves and (c) AFM results of machined grooves. 
Type Of Material Database/Collection of data 
Year Produced 2023 
Provided To Others? Yes  
Impact The novelty of the proposed method is that it combines two classical approaches for modelling the nonlinear behaviour of piezoelectric materials. More specifically, two sources of nonlinearity are considered simultaneously by combining the field-dependant model from Muller and Zhang with the frequency-dependant model from Damjanovic. The resulting combined model is employed to establish the piezoelectric constitutive equations implemented in the developed coupled field FE model. A further distinguishing characteristic of the work is that the proposed approach was subsequently validated by comparing the predicted widths of nanoscale grooves against those machined with a custom AFM-based vibration-assisted nanomachining configuration. 
URL http://doi.org/10.1016/j.ijmecsci.2022.108048
 
Title Comparison between torsional spring constants of rectangular and V-shaped AFM cantilevers - dataset 
Description This is the data set for a study on the comparison between torsional spring constants of rectangular and V-shaped AFM cantilevers. It comprises a number of related data sub-sets as follows: 1) Displacement and force data recorded experimentally for three different V-shaped cantilever models loaded with a normal force. These data were used to plot the graph shown in Figure 8 in the manuscript. 2) Displacement data simulated using Finite Elements (FE) models of pyramidal and prismatic tips attached to a rectangular cantilever and loaded with a lateral force. 3) Displacement and force data recorded experimentally for three different V-shaped cantilever models and the equivalent three rectangular cantilevers models. In all experiments, the cantilevers were loaded with a lateral force. These data were used to plot the three graphs shown in Figure 11 in the manuscript. 4) Three Finite Element (FE) models of rectangular cantilevers when loaded with a normal force. These models were prepared in accordance with the procedure described in section 3.2 in the manuscript. The theoretical values of the normal spring constant obtained with these FE models are presented in table 2 in the manuscript. 5) Finite Element models of two sets of equivalent rectangular and V-shaped cantilevers (i.e. four models in total) when loaded with a lateral force. These models were prepared in accordance with the dimensions of the experimental samples, which are given in the manuscript. 
Type Of Material Database/Collection of data 
Year Produced 2019 
Provided To Others? Yes  
URL https://research.cardiff.ac.uk/converis/portal/detail/Dataset/65547679?auxfun=<=en_GB