Revealing and Predicting the Failure Mechanisms in Advanced Materials for Energy - Enhancing Life and Efficiency

Lead Research Organisation: Imperial College London
Department Name: Mechanical Engineering

Abstract

The efficiency, safety and reliability of a wide range of engineering systems in the energy sector rely strongly on the performance of their structural components. Increasing energy efficiencies, achieved by maximising operating temperatures, will drive down CO2 emissions and is therefore essential to meet stringent legislation and the UK's and international short and long-term energy goals. Engineering components operate under adverse conditions (stress, temperature and harsh environments) causing their degradation and failure by deformation and fracture processes. Existing energy facilities are aging beyond design life and require life extension to secure short-term energy supplies. Reliable component lifetime assessment is therefore vital to ensure safe operation. New build nuclear reactors will soon be developed and future reactors designed for very high temperature operation and superior performance. Plans are also advanced for the construction of the next generation of conventional power stations with excess operating temperatures and efficiencies. Opportunities are now emerging to exploit a novel collection of innovative techniques, at micro and macro length scales, to obtain a fundamental understanding of material failure mechanisms. These will enable advanced materials and component designs with predictable in-service behaviour, which are crucial to innovation in the energy sector and the key for overcoming the outstanding challenges.Emerging experimental techniques can now reveal the processes, and quantify the extent of deformation and damage in a material as it occurs. High-energy X-ray tomography measurements will give detailed quantitative 3D volumetric insights of damage development, coalescence and failure mechanisms in the bulk of specimens at micro-length scales, during deformation under stress at temperature. In addition, complimentary non-destructive tools will be innovated for practical monitoring of large scale component degradation. At a range of length scales, a digital image correlation technique will be used to measure 3D surface strains on various geometries, and will provide evidence of the influence of defects and material inhomogeneities due to welding processes on strain fields and their evolution with time.High performance computing now facilitates advanced models to simulate material behaviour and structural components' response under various operating conditions. Experimental results will provide the basis for validated mechanistic models of material deformation and failure behaviour, which will be developed and incorporated into 3D computational models that can also include various regions of inhomogeneous material behaviour. This novel collection of advanced experimental techniques, combined with the verified computational models, will provide new powerful tools that are essential to understand and predict component failure, advance designs and optimise their operation.Initially, power plant steels will be examined. However, the methodologies developed can be extended to a wide range of materials relevant to e.g. aerospace, heat and power generation, marine and chemical technologies. The outcomes will lead to methods for component on-line monitoring, predictive multi-scale modelling of materials' initial and through-life properties and the development of accurate assessment procedures for component lifetime predictions that leads to the required plant life extension. Social and economical benefits include minimised environmental impacts, secure supplies, reduced maintenance costs and increased safety. The close collaboration with industry (including partners British/EDF Energy and E.ON) will provide an effective knowledge transfer mechanism between industry and academia, ensure industrial relevance and provide inspiration to a new generation of researchers. This fundamental, timely research is therefore valuable across industrial sectors in addition to the scientific community.

Planned Impact

The outcomes of this fellowship and its research findings will have social, economical and environmental impacts, in addition to direct industrial and academic benefits. The fundamental understanding of material deformation and failure mechanisms achieved through this research, and the reliable component lifetime prediction tools established, will lead to the development of advanced materials and component designs for energy applications. The increase in energy efficiency, achieved by enabling industrial plant components to operate at advanced temperatures in a safe and predictable manner, will reduce CO2 emissions and energy production costs. This will aid UK and international energy goals to be achieved and stringent legislation to be realised. Significant savings will be achieved through reduced component failures and maintenance costs. The research findings and methodologies developed in this work will lead to plant life extension, which relies on the assured, safe operation of their structural components. Subsequently, major concerns of energy shortfall in the imminent future will be addressed. The increase in operating efficiencies, reduced maintenance costs and energy security may also affect energy prices and thus industrial manufacturing costs. In the advent of a nuclear renaissance and the next generation of advanced conventional power stations with extreme operating temperatures and efficiencies, it is essential that we develop and retain capability and enhance expertise within the UK in this research field. Currently, there is a lack of such researchers, particularly young researchers, which are vital for the UK's future success and leadership in this research and commercial sector. The extensive industrial and research network that I have established will be exploited during this fellowship to provide vitally important mechanisms for knowledge transfer between academia and industry. This knowledge transfer will be realised through industrial collaborations, studentships developed in partnership with industry (especially the engineering doctorate (EngD) projects, which are set to produce the future industrial leaders) and widely disseminating the research internationally. I have established an excellent track record for research dissemination, including lectures on professional development courses, research forums, international conference presentations, invited talks, publications and a number of international network activities (see CV). In addition, opportunities to visit and extent collaborations with international research institutes will be exploited, to enhance international knowledge transfer. Furthermore, invitations to promote the research field and to encourage UK students to follow a career in science and engineering will be pursued, which will be of long-term benefit to the UK's capabilities. The research results will be of significant commercial benefit. Specifically, the advanced predictive techniques for damage and fracture can be developed into codes and software that are commercially exploitable to industry both nationally and internationally. I have already succeeded in incorporating my research findings into internationally recognised codes and standards (see CV). In addition, in-situ, remote plant component monitoring technologies will be developed through the innovative non-destructive evaluation techniques established during this research programme. The novel, experimental and predictive modelling techniques developed will be applicable to a range of materials. A wide range of industries will therefore benefit from this research, including aerospace, marine technology and petro-chemical processing. I have established extensive networks with these industries, providing effective routes for dissemination. Imperial has the mechanisms in place to exploit the technology and results developed through Imperial Innovations Ltd., the Imperial College London technology transfer company.

Publications

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Ahn J (2018) FEM prediction of welding residual stresses in fibre laser-welded AA 2024-T3 and comparison with experimental measurement in The International Journal of Advanced Manufacturing Technology

 
Description 1. Accurate laboratory measurements of crack initiation and growth are of vital importance for characterising material behaviour for use in the residual life assessment of structural components. The Potential Drop (PD) technique is one of the most common methods of performing these measurements, but such measurements are also sensitive to large inelastic strains which are often erroneously interpreted as crack growth. Despite the maturity of the PD technique, the extent of these errors is not fully understood and the most appropriate method of suppressing them is unknown. A finite element based tool has been developed which is capable of predicting the influence of strain on PD. Using this tool in conjunction with experimental measurements, performed using a novel low frequency ACPD system, it has also been demonstrated that some of the common methods currently used to interpret PD measurements during these tests are not fit for purpose when testing ductile materials. Alternative procedures to address this limitation have been developed. In addition the proposed method of interpreting creep crack growth data has been employed to re-validate the creep crack initiation prediction models provided in the EDF Energy defect assessment procedure R5.

2. A novel creep strain monitoring tool was validated in the laboratory through comparison of its results with that of other experimental techniques, including digital image correlation. Furthermore the experimental measurements were validated through comparison finite element analysis results. This validation on laboratory specimens was initially required and has been an important step in the tools deployment for creep strain monitoring in-situ on high temperature power plant components.

3. The influence of creep strain/damage on the mechanical response of 316H stainless steel, for use in UK advance gas cooled reactors AGRs, has been determined and partly quantified. The importance of developing a combined elastic-plastic-creep deformation model has been established and is has been put into development.
Exploitation Route The novel low frequency ACPD system developed, with its advanced accuracy, may now be employed by others requiring more accurate measurements of the onset of ductile/creep crack growth. The methodologies developed to interpret the PD response to during fracture toughness tests have been incorporated into ASTM E1820 -20 testing standard which is widely used by academic and industrial beneficiaries.

The novel creep strain monitoring tool developed and validated in the laboratory has been deployed and its results are currently being validated on high temperature plant components. This may be further used by industry to monitor and predict the onset of failure in power plant components.

The material model and assessment methodology developed may be used by others via its incorporation into assessment procedures as detailed in the Narrative Impact section.
Sectors Energy

 
Description Having been awarded a five year EPSRC career acceleration (2010-2015) in partnership with EDF Energy and E.ON, in addition to other research grant I hold in collaboration with industry, my research outcomes have had significant industrial impact both in the UK and internationally via the development structural assessment codes and testing standards, as described below. My research has had significant Industrial impact through its integration into testing codes and standards. My close collaboration with EDF Energy, who develop the high temperature defect assessment procedure the R5 Code, provides a direct route for industrial impact. The R5 code is used routinely for the lifetime assessment of UK nuclear plant and is employed worldwide in a range of industries for the assessment of components operating at high temperature. I have developed new analysis methods which were integrated into creep crack growth testing standards ASTM E1457-09 and the R5 Code. I have led research on the development of advanced electric potential difference methods to measure creep/ductile crack initiation and growth. Previous techniques were difficult to interpret as the effects of deformation and damage/crack initiation are often coupled, hence there was significant error and ambiguity associated with crack initiation measurements. The results of this novel work h have been incorporated into the ASTM 'Standard Test Method for Measurement of Fracture Toughness' ASTM E1820 and the creep crack growth testing standard ASTM E1457. In addition, based on my research on the development of creep crack growth test methods for welded geometries and research I co-supervised on the evaluation of fracture parameters for welded samples, an annex has recently (2013) been added to creep crack growth testing standard ASTM E1457 providing recommendations for testing specimens containing welds. I led two research projects (a ME3 design make and test, DMT, and an ME4 Individual project 2012-2014) at Imperial that have resulted in two novel self-loading rigs being developed that enable creep-fatigue tests to be performed on (i) round bar uniaxial or notched samples (i) homogenous and welded cantilever beam samples. These rigs have been recognised as an important solution to meet current needs for affordable, long term experimental testing in a range of environments have been exploited by collaborators including AMEC and EDF Energy. The research findings have been used to generate the required data to address EDF Energy's issues on environmental fatigue and the results used to advance the R5 assessment procedure. These codes and standards are adopted internationally and are vital to industry, and therefore contributions to them are a means of demonstrating the UK's leadership in this field. For example, the codes are critical for the operation of EDF Energy's Advanced Gas Cooled Reactors (AGR) nuclear plant to ensure the safety of the high temperature components prone to cracking and they play a very important part in presenting a case for lifetime extension of the UK's high temperature plant. The development of codes therefore has significant social and economic impact.
Sector Energy
 
Description Environmental Impact on the Structural Integrity of Nuclear Components (ENVISINC)
Amount £340,793 (GBP)
Funding ID 24462-167208 
Organisation Innovate UK 
Sector Public
Country United Kingdom
Start 04/2014 
End 03/2017
 
Description Feasibility Study into Additive manufacturing Processess for Alloys
Amount £30,000 (GBP)
Organisation Engineering and Physical Sciences Research Council (EPSRC) 
Sector Public
Country United Kingdom
Start 09/2013 
End 08/2014
 
Description Flexible and Efficient Power Plant: Flex-E-Plant
Amount £1,997,000 (GBP)
Funding ID EP/K021095/1 
Organisation Engineering and Physical Sciences Research Council (EPSRC) 
Sector Public
Country United Kingdom
Start 08/2013 
End 07/2017
 
Description HTC Support for PhDs and EngD Projects
Amount £116,020 (GBP)
Organisation EDF Energy 
Sector Private
Country United Kingdom
Start 10/2012 
End 09/2016
 
Description ICase EPSRC/Rolls-Royce
Amount £108,648 (GBP)
Organisation Rolls Royce Group Plc 
Department Rolls Royce Submarines
Sector Private
Country United Kingdom
Start 10/2014 
End 03/2018
 
Description Material Component Performance-driven Solutions for Long-Term Efficiency Increase in Ultra Supercritical Power Plants'
Amount £387,144 (GBP)
Funding ID 249809 
Organisation European Commission 
Sector Public
Country European Union (EU)
Start 06/2011 
End 02/2015
 
Description Potential Drop Monitoring of Creep Damage
Amount £284,148 (GBP)
Funding ID EP/J015431/1 
Organisation Engineering and Physical Sciences Research Council (EPSRC) 
Sector Public
Country United Kingdom
Start 07/2012 
End 06/2015