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TiPToP - TaIlored Pulse excitation for TailOred Plasma chemistries

Lead Research Organisation: University of Liverpool
Department Name: Electrical Engineering and Electronics

Abstract

Abstracts are not currently available in GtR for all funded research. This is normally because the abstract was not required at the time of proposal submission, but may be because it included sensitive information such as personal details.

Publications

10 25 50

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Dickenson A (2021) Electromechanical coupling mechanisms at a plasma-liquid interface in Journal of Applied Physics

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Gilbart B (2021) Dominant heating mechanisms in a surface barrier discharge in Journal of Physics D: Applied Physics

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Gilbart B (2022) Mutual interaction among multiple surface barrier discharges in Plasma Processes and Polymers

 
Description In this award a series of novel and highly tuneable nanosecond pulse plasma generators were developed to facilitate exploration of voltage pulse characteristics on the mean energy of electrons. Such efforts are an important first step to being able to control electron energy which would ultimately facilitate control over the generation and loss pathways of reactive plasma species that drive many applications spanning the domains of healthcare, manufacturing and energy.

We further developed a Laser Thomson Scattering (LTS) diagnostic system to enable the accurate time and space resolved measurements of electron temperature and density. This resulting facility is unique within the UK and is one of only a few available worldwide. A number of high impact papers have resulted from these efforts and the LTS technique has opened new research avenues to explore going forward.

By combining the advanced plasma chemistry diagnostics available in the York plasma institute with the nanosecond pulsed plasma sources and LTS facility available in Liverpool we were able to demonstrate, for the first time, that tailoring the voltage pulse shape has a significant impact on the mean energy of electrons in the plasma. This finding satisfies a key objective of the project.

A second objective of the research was to explore the impact of tailored pulse excitation on the reactive chemical species created by the plasma. To achieve this, we performed time and space resolved measurements using the ps-TALIF method of important atomic species (e.g. O, H and N) which are primarily generated via electron driven processes. Contrary to our expectations, the densities of these species did not show significant variation with voltage pulse shape. Through computational modelling, we were able to unravel the complex underpinning generation and loss pathways and demonstrate that build-up of O and H densities in a pulsed discharge continues after electron-impact dissociation processes have ceased. This build up is driven by additional afterglow processes, including dissociative recombination of O2+ and H2+. This is an important finding for the research community and highlights that a far greater focus and research effort should be devoted to afterglow processes, which are typically considered less important than electron-impact processes.
Exploitation Route Electron dynamics in a plasma are of fundamental importance. The insight gained thus far on the award contributes to our growing understand of electron behaviour in a non-equilibrium gas discharge. This information could be used by others to optimise plasma technology for use in domains such as healthcare, agriculture and manufacturing.
Sectors Agriculture

Food and Drink

Environment

Healthcare

Manufacturing

including Industrial Biotechology

 
Description Beyond academia the outcomes of this award have resulted in tangible economic impact. The plasma technology developed, diagnostic techniques established, and understanding gained on this award have enabled our plasma technology to be translated into the food processing sector to enhance food security and the sustainability of the UK food supply chain. Two patents were filed which were related to the technologies developed on this award. By exploiting this IP, the PDRA employed to work on the award, supported by the wider research team, secured ~£300,000 from Innovate UK and a further £260,000 from private investors to establish a spin-out company focused on using pulsed plasmas to eradicate chemical (e.g. allergens) and biological (e.g. bacteria) hazards from food processing surfaces. This highly efficient plasma-based approach to surface decontamination overcomes the need to halt food production for routine cleaning and thus offers manufacturers considerable time and energy savings. The company, Plasma Fresh ltd, is based at SciTech Daresbury and currently employs four people, including two former plasma scientists from the Liverpool research team. The research grant uncovered fundamental processes critical to controlling plasma technology, providing novel insights into plasma behavior and manipulation. These findings served as a springboard for further innovation and have been directly leveraged in two recently awarded EPSRC grants and an Innovate UK project. The new understanding of plasma control mechanisms not only demonstrates the scientific value of the original research but also drives ongoing advances in this technology's industrial and commercial applications.
First Year Of Impact 2023
Sector Agriculture, Food and Drink,Manufacturing, including Industrial Biotechology
Impact Types Economic

 
Description Beyond Bosch: On-farm fertiliser generation for net zero agriculture
Amount £800,000 (GBP)
Funding ID APP42644 
Organisation Engineering and Physical Sciences Research Council (EPSRC) 
Sector Public
Country United Kingdom
Start 06/2025 
End 06/2027
 
Description ICURe Exploit Funding FY23 Round 1
Amount £293,914 (GBP)
Funding ID 1007886 
Organisation Innovate UK 
Sector Public
Country United Kingdom
Start 09/2023 
End 10/2024
 
Description ICURe award
Amount £35,000 (GBP)
Funding ID I-I-003 
Organisation Innovate UK 
Sector Public
Country United Kingdom
Start 11/2022 
End 03/2023
 
Description Plasma-triggered Gelation
Amount £1,300,000 (GBP)
Funding ID APP13486 
Organisation Engineering and Physical Sciences Research Council (EPSRC) 
Sector Public
Country United Kingdom
Start 03/2025 
End 03/2028
 
Title Decontamination of Food by Plasma 
Description Description of a technique to manipulate plasma species for the purpose of microbial decontamination 
IP Reference P44601GB1 
Protection Patent / Patent application
Year Protection Granted 2023
Licensed No
Impact Used as the basis for a spin-out company.
 
Title Low temperature plasma for the removal of airborne contamination 
Description Patent on plasma based system to degrade organic contamintion in air flows. 
IP Reference GB2208962.7 
Protection Patent / Patent application
Year Protection Granted 2022
Licensed No
Impact Is forming the basis of a spibn-out company.
 
Company Name PlasmaFresh 
Description PlasmaFresh develops decontamination solutions for the food and drink manufacturing industry, using cold plasma technologies. 
Year Established 2023 
Impact The company has raised over £600k from Innovate UK and STFC and is currenlty based at SciTech Daresbury. The company employs a former EPSRC funded PhD student and an EPSRC funded PDRA.
Website https://plasmafresh.co/