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Novel microcapsule designs and manufacturing processes

Lead Research Organisation: UNIVERSITY OF CAMBRIDGE
Department Name: Chemical Engineering and Biotechnology

Abstract

Abstracts are not currently available in GtR for all funded research. This is normally because the abstract was not required at the time of proposal submission, but may be because it included sensitive information such as personal details.

Publications

10 25 50

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Lobel BT (2025) Nonspherical Particle Stabilized Emulsions Formed through Destabilization and Arrested Coalescence. in Langmuir : the ACS journal of surfaces and colloids

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Al-Sharabi M (2024) Magnetic zinc oxide/silica microbeads for the photocatalytic degradation of azo dyes in Colloids and Surfaces A: Physicochemical and Engineering Aspects

 
Description We have been making spherical and non-spherical microparticles that contain an oil core and an inorganic shell. These materials can be used in laundry detergents and the fragrance or enzyme only released when desired. We have been making silica microbeads via a templated aggregation mechanism and we are putting a polymeric shell around the bead. We are measuring the adhesion of the beads onto different surfaces as well as the force necessary to crush them
Exploitation Route Six papers have been published from this project with a seventh currently under review. There is a review paper which covers the entire area and a range of exemplar appers for specific systems that show non-spherical capsules through to vitamin encapsulation. The grant was a big success and was very productive.
Sectors Agriculture

Food and Drink

Chemicals

Energy

Manufacturing

including Industrial Biotechology

Pharmaceuticals and Medical Biotechnology

 
Description Infineum UK Ltd 
Organisation Infineum International
Country United Kingdom 
Sector Private 
PI Contribution Innovative company who make engine oil additives and are looking to diversify.Looking at how encapsulatio can aid their product range We are looking at friction modification using neutron reflectivity at the ISIS neutron source and use a custom built tribometer which was designed and paid for by Infineum - we have aso benefitted from proprietary Infineum purchased beamtime as well as peer reviewed time - encapsulation as investigated in this project is a clever way to contriol friction evolution over time
Collaborator Contribution Knowledge of encapsulaion and demonstration of antioxidant and rheological control encapsulation
Impact Alexander J. Armstrong, Thomas M. McCoy, Rebecca J. L. Welbourn, Robert Barker, Jonathan Rawle, Beatrice Cattoz, Peter J. Dowding, and Alexander F. Routh, Towards a high-shear neutron and X-ray reflectometry environment for the study of surface-active materials at solid-liquid interfaces, Scientific Reports 11:9713 2021 Alexander J. Armstrong, Rui F. G. Apostolo, Thomas M. McCoy, Finian J. Allen, Rebecca J. L. Welbourn, James Doutch, Beatrice N. Cattoz, Peter J. Dowding, Alexander F. Routh, and Philip J. Camp, Experimental and Simulation Study of Self-Assembly and Surface Adsorption of Glycerol Monooleate in n-Dodecane onto Iron Oxide. Nanoscale 16: 1952-1970 2024.
 
Description Olivier Cayre at leeds 
Organisation University of Leeds
Country United Kingdom 
Sector Academic/University 
PI Contribution The project is a collaboration between Leeds, Birmingham and Cambridge
Collaborator Contribution Three post-docs all working closely together
Impact Mohammed Al-Sharabi, Daniele Baiocco, Benjamin T. Lobel, Olivier J.Cayre, Zhibing Zhang and Alexander F. Routh, Magnetic Zinc Oxide/Silica Microbeads for the Photocatalytic Degradation of Azo Dyes, Colloids and Surfaces A 695:134169 2024. Daniel Baiocco, Benjamin Lobel, Mohammed Al-Sharabi, Olivier J. Cayre, Alexander F. Routh, Zhibing Zhang Environmentally Friendly Calcium Carbonate-Polydopamine Microcapsules with Superior Mechanical, Barrier, and Adhesive Properties, Sustainable Materials and Technologies 41: e01001 2024. Daniele Baiocco, Mohammed Al-Sharabi, Benjamin Lobel, Olivier J. Cayre, Alexander F. Routh, Zhibing Zhang, Eco-Friendly Fungal Chitosan-Silica Dual-Shell Microcapsules with Tailored Mechanical and Barrier Properties for Potential Consumer Product Applications, ACS Omega 9(26): 28385-28396 2024, Benjamin T. Lobel, Daniele Baiocco, Mohammed Al-Sharabi, Alexander F. Routh, Zhibing Zhang and Olivier J. Cayre, Current Challenges in Microcapsule Designs and Microencapsulation Processes: A Review, ACS Applied Materials and Interfaces 16 (31): 40326-40355 2024. Benjamin T. Lobel, Daniele Baiocco, Mohammed Al-Sharabi, Alexander F. Routh, Zhibing Zhang, Olivier J. Cayre, Non-spherical particle stabilised emulsions formed through destabilisation and arrested coalescence, Langmuir 41(1): 550-562 2025. Mohammed Al-Sharabi, Benjamin T. Lobel, Daniele Baiocco, Olivier J. Cayre, Zhibing Zhang and Alexander F. Routh, Multicore Silica Microcapsules Containing a-Tocopherol for Potential Consumer Product Applications, Materials Advances, 6:1468 - 1477 2025. Dan Baiocco, Benjamin Lobel, Mohammed Al-Sharabi, Olivier Cayre, Alexander Routh and Zhibing Zhang, Organic-Inorganic Multi-layer Microcarriers with Superior Mechanical Properties for Potential Active Delivery in Fast-Moving Consumer Goods, Industrial & Engineering Chemistry Research 64 (9) : 4917-4931 2025.
Start Year 2021
 
Description Zhibing Zhang at Birmingham 
Organisation University of Birmingham
Department School of Chemical Engineering
Country United Kingdom 
Sector Academic/University 
PI Contribution Three postdocs all working closely together
Collaborator Contribution Project is a collaborationb between Leeds, Birmingham and Cambridge
Impact Mohammed Al-Sharabi, Daniele Baiocco, Benjamin T. Lobel, Olivier J.Cayre, Zhibing Zhang and Alexander F. Routh, Magnetic Zinc Oxide/Silica Microbeads for the Photocatalytic Degradation of Azo Dyes, Colloids and Surfaces A 695:134169 2024. Daniel Baiocco, Benjamin Lobel, Mohammed Al-Sharabi, Olivier J. Cayre, Alexander F. Routh, Zhibing Zhang Environmentally Friendly Calcium Carbonate-Polydopamine Microcapsules with Superior Mechanical, Barrier, and Adhesive Properties, Sustainable Materials and Technologies 41: e01001 2024. Daniele Baiocco, Mohammed Al-Sharabi, Benjamin Lobel, Olivier J. Cayre, Alexander F. Routh, Zhibing Zhang, Eco-Friendly Fungal Chitosan-Silica Dual-Shell Microcapsules with Tailored Mechanical and Barrier Properties for Potential Consumer Product Applications, ACS Omega 9(26): 28385-28396 2024, Benjamin T. Lobel, Daniele Baiocco, Mohammed Al-Sharabi, Alexander F. Routh, Zhibing Zhang and Olivier J. Cayre, Current Challenges in Microcapsule Designs and Microencapsulation Processes: A Review, ACS Applied Materials and Interfaces 16 (31): 40326-40355 2024. Benjamin T. Lobel, Daniele Baiocco, Mohammed Al-Sharabi, Alexander F. Routh, Zhibing Zhang, Olivier J. Cayre, Non-spherical particle stabilised emulsions formed through destabilisation and arrested coalescence, Langmuir 41(1): 550-562 2025. Mohammed Al-Sharabi, Benjamin T. Lobel, Daniele Baiocco, Olivier J. Cayre, Zhibing Zhang and Alexander F. Routh, Multicore Silica Microcapsules Containing a-Tocopherol for Potential Consumer Product Applications, Materials Advances, 6:1468 - 1477 2025. Dan Baiocco, Benjamin Lobel, Mohammed Al-Sharabi, Olivier Cayre, Alexander Routh and Zhibing Zhang, Organic-Inorganic Multi-layer Microcarriers with Superior Mechanical Properties for Potential Active Delivery in Fast-Moving Consumer Goods, Industrial & Engineering Chemistry Research 64 (9) : 4917-4931 2025.
Start Year 2021