ASAP - Advanced electromagnetic Sensors for Assessing Property scatter in high value steels

Lead Research Organisation: University of Manchester
Department Name: Electrical and Electronic Engineering

Abstract

The development of new techniques to measure the microstructure of a material in a non-contact non-destructive fashion can lead to a dramatic improvement in the understanding of the material and its behaviour during processing and in-service. This, in turn, can lead to a greater ability to control the material properties and predict the evolution of these properties. At present, the majority of microstructural analysis techniques are destructive and / or require small samples. Consequently, existing techniques are limited in applicability especially if dynamic microstructural control during commercial processing is of interest. Several techniques have been proposed to directly measure microstructures in these situations but, as yet, no single technique offers a full solution. It is well known that the microstructure is directly related to the mechanical properties of steel, therefore if the microstructure can be measured on-line during processing, and the inherent variability in microstructure can be assessed (on-line or off-line), then the mechanical properties (including any scatter) can be inferred. This could provide enormous saving to the manufacturing industry as product quality can be improved through real-time feedback for processing control and / or reduction (or better still elimination) of the off-line destructive mechanical testing for release specifications. In this context, our proposal focuses directly on advanced sensors for measuring the key microstructural parameters that are directly linked to mechanical properties in high value steels.

Our ambition is to exploit novel electromagnetic (EM) techniques to analyse microstructure directly, and therefore to infer mechanical properties, for a range of advanced steel types during and after processing. Typically these EM techniques have included multi-frequency interrogation combined with advanced signal and data processing and modelling. Both the UK and Indian teams have successfully considered the electromagnetic response, using different sensor types, to component phase fractions (such as ferrite), which in the UK has been supported by 3D modelling of both idealised and realistic microstructures. In parallel, the problem of inverting the complex inductance spectra acquired by the sensor systems to yield parameters of metallurgical significance has been addressed, and in India a link between sensor output and mechanical properties for relatively simple steels has been established. In the EU sensor configurations that can be deployed on-line for phase transformation monitoring by measuring the mutual inductance have been successfully tested, in collaboration with Tata Steel Europe, and are now in the process of being commercially exploited via a licensing agreement with an external company. The natural next step in the research is to combine EM sensor techniques to exploit the full electromagnetic characteristics of steel (for example using sensors that measure coercivity, saturation and incremental permeability) to characterise the more complex microstructures, and their spatial inhomogeneity, in advanced steels. This requires collaboration between the leading international groups on sensor design, implementation and microstructure-signal relationships. On-line deployment of these systems will allow greater feedback control during processing to enable these advanced steels to be produced on older as well as new mills. Mechanical property determination, through the microstructure-property relationships, provides the potential to reduce or eliminate the off-line property release tests that are currently performed with a significant saving to the industry.

Planned Impact

The potential beneficiaries of this project may be grouped in the following categories:

Society
Environmental
Industrial (steel producers, steel end users, support organisations etc)
Academic and scientific

In the broadest sense, the industrial benefits will stem from an ability to provide reliable inspection technologies, in-service, for high value steels especially with the need for non-destructive measurement of materials properties (including scatter) for release testing and on-line process control. Greater on-line processing control will enable to production of higher strength/formability strip product that can be used to further lightweight car bodies. There is then an environmental and societal benefit in terms of increased efficiency (lower fuel consumption) and reductions in CO2 emissions.

Although this project focuses on steel processing mills, which has very high industrial, environmental and global importance, the research is also highly inter-disciplinary, and involves a variety of areas such as: metallurgy, electromagnetic engineering, magnetism, modelling and simulation, electronics, digital signal processing, inverse algorithms, process and mechanical engineering and applied mathematics. In general, results from the project will be beneficial to a cross-section of scientific workers in these areas and we would reasonably expect spin-off applications to arise in other areas, as we have seen from the previous work we have done.

Academics working on materials characterisation will benefit from the development of a non-destructive sensor that can monitor microstructures. Greater knowledge of EM signal - microstructure relationships will benefit the NDT community.

Publications

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Description The development of new techniques to measure the microstructure of a material in a non-contact non-destructive fashion can lead to a dramatic improvement in the understanding of the material and its behaviour during processing and inservice. This, in turn, can lead to a greater ability to control the material properties and predict the evolution of these properties. At present, the majority of microstructural analysis techniques are destructive and / or require small samples. Consequently, existing techniques are limited in applicability especially if dynamic microstructural control during commercial processing is of interest. Several techniques have been proposed to directly measure microstructures in these situations but, as yet, no single technique offers a full solution. It is well known that the microstructure is directly related to the mechanical properties of steel, therefore if the microstructure can be measured on-line during processing, and the inherent variability in microstructure can be assessed (on-line or off-line), then the mechanical properties (including any scatter) can be inferred. This could provide enormous saving to the manufacturing industry as product quality can be improved through real-time feedback for processing control and / or reduction (or better still elimination) of the off-line destructive mechanical testing for release specifications. In this context, our proposal focuses directly on advanced sensors for measuring the key microstructural parameters that are directly linked to mechanical properties in high value steels.

This project has helped to develop novel electromagnetic (EM) techniques to analyse microstructure directly, and therefore to infer mechanical properties, for a range of advanced steel types during and after processing. The sensor exploit multi-frequency interrogation combined with advanced signal and data processing and modelling. The sensors have been deployed on-line for phase transformation monitoring by measuring the mutual inductance,in collaboration with Tata Steel Europe, and are now being commercially exploited via a licensing agreement with Primetals Technologies.
Exploitation Route The next step is to "close the loop" in the engineering of advanced high strength steels by using the sensor outputs to control process parameters during hot rolling, such as the flow of cooling water. These are being addressed in a follow on EPSRC project (Real-time In-line Microstructural Engineering) and major EU project involving approximately 15 partners - OMA (On line Microstructure Analytics) amd commercially in partnership with Primetals Technologies
Sectors Energy,Manufacturing, including Industrial Biotechology

 
Description Industrial contribution to UK & India Partnership in Advanced Manufacturing Research Challenges
Amount £75,000 (GBP)
Organisation Primetals technologies ltd 
Sector Private
Country United Kingdom
Start 03/2014 
End 02/2017
 
Description Real-time In-line Microstructural Engineering (RIME)
Amount £511,339 (GBP)
Funding ID EP/P027237/1 
Organisation Engineering and Physical Sciences Research Council (EPSRC) 
Sector Public
Country United Kingdom
Start 07/2017 
End 12/2020
 
Description Alstom - contribution to PowerEMS and ASAP 
Organisation Alstom
Department Alstom UK
Country United Kingdom 
Sector Private 
PI Contribution Project partners in the PowerEMS and ASAP projects
Collaborator Contribution Supply of samples and expertise.Facilitating access to technical resources
Impact Progress on understanding the response of P90 type steels, which are widely used in the power industry, to electromagnetic sensors. Realization of demonstration systems.
Start Year 2009
 
Description E On - contribution to PowerEMS and ASAP 
Organisation E ON
Country Germany 
Sector Private 
PI Contribution Project partners in the PowerEMS and ASAP projects
Collaborator Contribution Supply of samples and expertise. Site visits and facilitating access to technical resources
Impact Progress on understanding the response of P90 type steels, which are widely used in the power industry, to electromagnetic sensors. Realization of demonstration systems.
Start Year 2009
 
Description EM microstructure monioring technology 
Organisation Primetals technologies ltd
Country United Kingdom 
Sector Private 
PI Contribution The company are a licencing partner
Collaborator Contribution Intellectual property - patents / know-how
Impact Commercialisation of sensor technology. The technology has now been licenced to Primetals, who have developed a commercial version and are now marketing the system. The hot strip mill at IJmuiden Hot strip mill a reference site for demonstrating the technology to the industry.
Start Year 2011
 
Description ETD - MPA tests 
Organisation European Technology Development (ETD Consulting)
Country United Kingdom 
Sector Private 
PI Contribution Evaluation of new electromagnetic micro structure sensors on aged P91 and P92 steel pipes at MPA in Stuttgart.
Collaborator Contribution Access to test facilities and the results from other partner's test methods during the tests
Impact Results to demonstrate the potential feasibility of the new electromagnetic sensor technology developed during ASAP. The collaboration started during the ASAP project and developed during RIME resulting in a series of site tests and future iterations of the sensor technology.
Start Year 2015
 
Description PowerEMS - Tata Steel 
Organisation Tata Steel Europe
Country United Kingdom 
Sector Private 
PI Contribution Project partners in the PowerEMS project
Collaborator Contribution Project partners in the PowerEMS project - supply of materials and expertise
Impact Longstanding multidisciplinary collaboration to apply the sensors developed during EPSRC project to steel production processes