Video microscopy of granular deformation and strain localisation in partially-solid alloys

Lead Research Organisation: Imperial College London
Department Name: Materials

Abstract

This project seeks to use video microscopy to observe and measure, for the first time, the deformation mechanisms in partially-solid alloys. The focus is on one of the least studied areas of mushy-zone mechanics, rheology at 'intermediate' solid fraction, when multiple equiaxed crystals are in contact but have negligible cohesion. These microstructures are commonly deformed during industrial casting processes, for example the high-pressure die-casting of Al- and Mg-alloy automotive chassis components. It has been found that, when severe deformation occurs at the same time as solidification, the as-cast microstructure and defects are markedly different to those in most textbooks. Recent research has suggested that this is because deformation during solidification causes the alloy to deform as a granular material.Granular materials are simply the disordered assemblies of particles we encounter every day from the soil in the garden to salt on the kitchen table. However, the mechanics of granular materials can be complex, emerging from the mechanical interactions between discrete particles which are often unrelated to the mechanics of the particles themselves. For example, grains of wheat in a silo have markedly different mechanical properties to the grains of sand in a soil, yet the deformation behaviour of large piles of each share many mechanical similarities. Granular materials are important across the physical sciences and engineering and the application of granular mechanics is central to research on (i) soil mechanics in Civil Engineering, (ii) plate tectonics and earthquakes in Earth Science, (iii) the flow and storage of cereal crops in Agriculture, and (iv) the handling of pharmaceutical powders and pastes in Chemical Engineering. This Project seeks to provide direct experimental proof that partially-solid alloys should also be considered a form of granular material. The ultimate aim is for the phenomena and mechanisms revealed by video-microscopy to form the foundation for future granular theories of partially-solid alloy deformation.To enable these scientific advances, an innovative apparatus for the direct in-situ measurement of deformation in the mushy-zone will be developed. The approach is to simultaneously measure (i) phenomena at the scale of the crystals in-situ and (ii) global mechanical data. The knowledge of granular deformation from the parallel disciplines of Soil Mechanics and Earth Science will be used in developing the apparatus and in interpreting the results. The research will generate knowledge of the deformation mechanisms operating at the scale of the crystals, and quantitatively link the micromechanisms with the global rheology. Research will also study how granular shear bands form and grow in partially-solid alloys.

Publications

10 25 50
 
Description (1) techniques for the synchrotron radiography of shear deformation in semi-solid alloys were developed. These techniques are applicable to Al- and Fe- based alloys and enable the direct measurement of semi-solid deformation mechanisms.

(2) the research provided direct evidence of shear-induced dilation in semi-solid alloys and, therefore, indicates that a granular approach (similar to that used in particulate materials such as soils) may be a useful way to consider semi-solid metals (both conceptually and in modelling).

(3) to deliver this project, a collaboration was developed between metallurgists, civil engineering researchers, X-ray imaging researchers, and adaptive machine systems engineers.. This collaboration continues today.
Exploitation Route The main academic finding is that shear-induced dilation plays a key role in the deformation of semi-solid alloys. With this evidence, the project has identified the need to reinterpret some of the literature on semi-solid alloy deformation and raises questions about whether past work has correctly interpreted the mechanisms underpinning semi-solid alloy deformation.

Although the findings of the project were on basic mechanisms in small samples, it is expected that the same mechanisms operate in industrial casting processes such as high-pressure die casting (HPDC) and twin-roll casting (TRC). With further development, the results could be taken forward to improve process models of HPDC and TRC which are key manufacturing processes used in the UK.
Sectors Aerospace, Defence and Marine,Manufacturing, including Industrial Biotechology

URL http://www.imperial.ac.uk/people/c.gourlay/research.html
 
Description Royal Society of London
Amount £12,000 (GBP)
Funding ID IE110386 
Organisation The Royal Society 
Sector Charity/Non Profit
Country United Kingdom
Start 02/2012 
End 02/2014
 
Description Royal Society of London
Amount £12,000 (GBP)
Funding ID IE110386 
Organisation The Royal Society 
Sector Charity/Non Profit
Country United Kingdom
Start 02/2012 
End 02/2014
 
Description Yasuda-sensei 
Organisation University of Kyoto
Department Department of Materials Science and Engineering
Country Japan 
Sector Academic/University 
PI Contribution Our research team have developed image processing and analysis approaches to quantify the synchrotron imaging datasets generated by Prof. Yasuda and his team at Kyoto University, and also developed models based on the synchrotron datasets.
Collaborator Contribution Prof. Yasuda and his team have developed the apparatus and adaptive machine systems required for synchrotron imaging at SPring-8. They have also contributed significantly to the analysis and interpretation of data.
Impact The outputs have been Journal papers and the advances in knowledge that they contain
Start Year 2013