Preform Rare-Earth Profiler (PREP)

Lead Research Organisation: University of Southampton
Department Name: Optoelectronics Research Centre (ORC)

Abstract

Over the last decade, high power fibre amplifiers and lasers have been rapidly developed and successfully commercialized for a number of industrial applications such as cutting, welding, and marking. The industrial fibre laser business is currently worth over $800M/year, with compound annual growth rate of about 13% - the highest among the different laser technologies. One of the main contributors to this success has been the significantly improved rare-earth doped fibre fabrication technologies.

High performance fibres rely on controlled incorporation of refractive index modifying dopants, as well as, gain providing rare-earth ions. High efficiency, high average and/or peak power industrial fibre lasers and amplifiers invariably use large-mode area fibres with complex refractive indices and rare-earth distributions. In most cases, a number of different dopants are used simultaneously in order to control the refractive index and gain distribution, and through it the fibre modality and modal differential gain. Additional dopants are also used to reduce nonlinear effects, such as Stimulated Brillouin and Raman Scattering, and other parasitic effects, such as photodarkening. The various dopants have different sizes, mobility, and diffusion rates and, as a consequence, the resulting refractive index profiles can in general be much different to rare earth distributions within the core, and one cannot be inferred from the other. In addition, depending on the fabrication technique, the distribution of dopants is not uniform along the fibre preform, rendering the drawn fibre performance variable and "patchy". In particular, Modified Chemical Vapour Deposition (MCVD) fabrication technique, among the most versatile and widely used fabrication techniques, is known to suffer from poor repeatability and large variability along the preform length. This compromises significantly the fibre yield and increases the fibre cost. In addition, and even more importantly, currently there is no reliable information regarding the "fitness-for-purpose" of fibre in advance. Its suitability can only be tested and quantified after a full fibre laser has been built and thoroughly tested, adding considerably to the fibre laser module turn-around time, yield and cost. So there is a need for unsuitable preforms or parts of preform to be identified early in the fibre drawing process and be discarded.

Another requirement has lately appeared in the fibre telecom area. Over the last few years there has been a strong resurgence in multimode telecom systems research, with spatial-division multiplexing (SDM) promising to solve the predicted forthcoming telecom capacity crunch. Successful development of SDM systems relies exclusively on the development of high performance multimode fibre amplifiers with carefully optimized rare-earth (Erbium or Thulium) profiles for modal gain equalization. Again, detailed and accurate knowledge of the active dopant distribution over the fibre cross-section along the entire preform length is critical for successful demonstrations of this game-changing approach to single-fibre transmission capacity increase.

The main aim of this proposal is to develop widely applicable, non-destructive characterization techniques for the accurate and detailed determination of active-dopant distribution in fibre preforms and provide the required reliable information well before the preforms are drawn into fibres. Such preform characterization techniques are expected to have a big impact on the performance and cost of advanced high-power fibre laser systems, as well as, currently researched SDM telecom systems, and increase the competiveness of the UK manufacturing basis as well as enhance the UK cutting-edge research activities in these areas.

Planned Impact

The PREP instrument will reveal fine detail about the preform designs being used by these companies. As such, many of the measurement results will be highly commercially sensitive. Confidential arrangements will therefore need to be put in place to protect 3rd party preform data and equally to protect participating companies' background know-how. However, this is not expected to restrain the delivery of impact as there are many preform designs being developed within the ORC, and the results from these will be published in journals, in conferences and seminars.

Specific activities to deliver impact include:

a) Existing industrial partners and academic collaborators will have direct access to technical data and progress, through the bi-annual technical meetings. Also the active participation of SPI's CTO and ORC Deputy Director in the MST will ensure proper alignment with both organisation needs.

b) Wider circle of potential users will be reached by publication of key results in international conferences (CLEO, Photonics West, OFC, ECOC) and high impact open-access journals (e.g. Optics Express and IEEE Photonics Journal).

c) Strong engagement with the University RIS team (through the ORC dedicated collaboration manager) to promote results and seek more collaborators for further exploitation of successful results.

d) Working closely South-East Photonics Network (SEPNET) manager (Dr. John Lincoln) to reach out to the >200 network members specialising in Photonics.

The most immediate metric for determining the success of the strategy in delivering value to industrial partners is the expected step change in active fibres and fibre laser modules yield, as well as, fibre laser optical and wall-plug efficiency increases.

The ability to pre-select only "fit-for-purpose" sections of preforms is expected to more than double the current fibre yield, and increase the laser efficiency close to the theoretical limit. Such advances are expected to increase fibre laser wall-plug efficiency from the current ~30% to over 45% - a level that cannot be reached by other laser technologies. In addition, the anticipated high power laser system yield is expected to reach >95% levels. Such performance improvements will reduce cost and increase further the fibre laser market penetration.

In the case of academic collaborators, the most appropriate metric of success is the number of high impact factor publications/conferences and contributions to future research grants/contracts that such novel instrument undoubtedly will enable.

However, there is an additional aim of the project in that it is desirable a commercial instrument to become available within five years that is reliable, robust, and which can be properly calibrated. Prerequisites include: research excellence in order to ensure that the best design approach is taken; good market feedback from the collaborators and other service recipients of the measurement technique; selection of the most appropriate commercialization route; and appropriate licensing of technology.
 
Description We have demonstrated that the basic principle is sound and provides accurate full preform characterisation data that can be used to pre-screen fibre preforms and increase the fibre laser manufacturing yield. We have also demonstrated that in order to fully and accurately exploit the measurements, the fluorescence data have to be correlated with additional data regarding the preform refractive index distribution.
The set up has been augmented in order to provide the refractive index data and locate the dopant distribution accurately within the refractive index profile.
The instrumentation has been augmented further and now provides the actual dopant concentration without destroying the preform. Such information was possible only with alternative destructive methods before.
In addition, the apparatus now provides high quality images of the core structure revealing the presence of non-uniformities and other irregularities that can potentially degrade the fibre laser performance. Such valuable information is not available by conventional commercially available preform characterisation apparatuses.
Exploitation Route We are in close collaboration with the supporting company and the new findings and improvements have been transferred into their measurement system and are currently used in the fibre production line. This has reduced considerably the preform optimisation time cycles and has increased the overall fibre yield. Such valuable information is not available by conventional commercially available preform characterisation apparatuses.
Sectors Aerospace, Defence and Marine,Digital/Communication/Information Technologies (including Software),Education,Manufacturing, including Industrial Biotechology

 
Description The first version of the instrument has been replicated and transferred to the supporting company (SPI Lasers) in order to characterise dopant distributions in their commercial preforms. The second version of the instrument is capable of providing absolute values of dopant concentrations in the preform core non-destructively. This has proven extremely important for the industrial collaborator. As a result of this advanced preform characterisation technique, the fibre laser efficiency has increased from ~25% to >35%, a significant improvement resulting in ~28% reduction the required pump diode power. The third version of the equipment, which combines rare-earth dopant concentrations and refractive index profiles has now been transferred to the industrial partner and used to characterise preforms internally
First Year Of Impact 2019
Sector Manufacturing, including Industrial Biotechology
Impact Types Economic

 
Description RAEng Chair and Advanced Laser Lab
Amount £247,000 (GBP)
Funding ID SP2001/N 
Organisation SPI Lasers UK 
Sector Private
Country United Kingdom
Start 09/2019 
End 08/2020
 
Title Advanced Fibre Preform Characterisation Tool 
Description This device is now fully integrated into SPI Lasers' fibre fabrication facilities and used to characterise preforms for high power fibre lasers and amplifiers 
Type Of Material Improvements to research infrastructure 
Year Produced 2020 
Provided To Others? No  
Impact As a result of this advanced preform characterisation technique, the fibre laser efficiency has increased from ~25% to >35%, a significant improvement resulting in ~28% reduction the required pump diode power. 
 
Title Preform Core and Pedestal Refractive Index characterisation apparatus 
Description Optical imaging set-up which provides high quality images of the optical preform core structure. 
Type Of Material Improvements to research infrastructure 
Year Produced 2018 
Provided To Others? Yes  
Impact The apparatus provides high quality images of the core structure in addition to information of the refractive index distribution. This additional information is not available by commercial refractive index profilometers. The information is critical in identifying parts of the preform that can potentially be limiting severely the fibre laser performance at a very early stage, thus avoiding unnecessary production steps and saving manufacturing time and costs. 
 
Title Preform Dopant Distribution Research Tool 
Description This version of the research tool provides extremely useful information about the dopant distribution in fibre preforms. In contrast with traditional methods, this tool provides non-destructive measurements and enables the use of the preform after characterisation. 
Type Of Material Improvements to research infrastructure 
Year Produced 2017 
Provided To Others? Yes  
Impact The first version of the tool has already been available to other fibre fabrication groups in the ORC and the supporting company (SPI Lasers) and has a positive impact on the active preform screening. This technique has now been extended to provide nondestructive information about the Refractive index and Dopant Profile as well as the absolute dopant concentration. The technique has been transferred to the supporting company. 
 
Title apparatus and software to determine independently the actual level of dopant concentration in doped optical preforms in a non-destructive manner. 
Description This novel apparatus uses bi-directional dual pump illumination technique to measure the actual dopant concentration level inside the optical preform core. This is achieved by consecutively using one-sided pump illumination and using the asymmetric absorption profiles to extract unambiguously the actual dopant concentration level. 
Type Of Material Improvements to research infrastructure 
Year Produced 2018 
Provided To Others? Yes  
Impact This research tool is unique in providing the actual level of the laser dopant concentration inside the preform core, in addition to the relative dopant distribution profile. Currently there is no commercial apparatus providing this extremely useful information in situ and non-destructively. This unique apparatus saves substantial amount of preform optimisation time. 
 
Description preform testing 
Organisation SPI Lasers UK
Country United Kingdom 
Sector Private 
PI Contribution Extensive testing of specially made experimental preforms and data analysis. The collaboration was extended to measure relative distributions as well as absolute values of dopant concentration in experimental advanced preforms
Collaborator Contribution preparation of two special preforms in order to test the accuracy of the testing equipment. provision of additional preforms to test the accuracy of absolute dopant concentration measurements
Impact Valuable data regarding the refractive index distribution and active dopant distribution inside advanced optical preforms with very complex distributions. Measurement of absolute values of dopant concentration without destroying the preform
Start Year 2016