Real-time In-line Microstructural Engineering (RIME)

Lead Research Organisation: University of Warwick
Department Name: WMG

Abstract

Steel continues to be the most used material in the world by value and play an essential role in all aspects of society, from construction to transport, energy generation to food production. The long-term sustainability of UK steel making requires lower energy production and the development of high value steel products. The ability to measure the microstructure of steel in a non-contact, non-destructive fashion can lead to dramatic improvement in the understanding of the material and its behaviour during processing and in-service. Improved control during processing will increase efficiency in production of complex steel microstructures and allow new generation alloys to be made. Through our previous EPSRC and industry funded research we have created a new electromagnetic (EM) measurement system, EMspecTM, that can monitor the microstructure of strip steel during hot processing. This system is now providing information related to the condition (transformed phase fraction) of the microstructure over 100% of the strip length. The scene is now set to make the next major step forward with the information that new in-line microstructure measurement systems can offer - proposed real-time in-line microstructural engineering, or 'RIME' technology.
Our ambition is to enable real-time microstructure engineering during processing via dynamic control of cooling strategies or heat treatment using EM sensor feedback, in particular to engineer microstructures that were previously either impossible to achieve in full scale production or could not be reliably achieved. This will require detailed knowledge of the full temperature - magnetic - microstructure parameter space and sensors that are capable of operating in elevated temperature environments (such as heat treatment facilities), which are not currently available outside the laboratory. In addition application to a wide range of product lines, from strip to plate or sections requires integration of through thickness cooling models and EM signal-depth interpretation all mapped for varying temperature and phase fraction. In this project we will develop new sensors that can operate at high temperature; both laboratory systems to determine full magnetic properties with temperature for model and commercial steels, essential information that is currently unavailable in the literature, and robust deployable sensors for trials in industrial conditions; and systems designed to interrogate for through thickness data. We will develop a demonstration facility, consisting of a furnace, run out table with cooling sprays and EMspecTM system, to allow dynamic feedback control of cooling schedules from EM sensor signals to engineer specific microstructures. Alongside the hardware and demonstration activities we will also develop modelling capabilities, both for sensor design and signal interpretation: our current models are used to relate sensor signals to microstructure (phase fraction and grain size at room temperature) with incorporation of temperature effects planned in this project. A number of case studies have been identified to trial the new technologies including advanced high strength strip steels (AHSS) for light-weighting of vehicles, high strength - high toughness pipeline steels for demanding environments, high strength, more uniform, constructional steels and tailoring microstructure in rod.

Planned Impact

This project aims to develop electromagnetic sensing technology to allow real-time in-line microstructural engineering for steels to give increased efficiency processing and enable production of new advanced high strength strip (AHSS) steel grades. The main benefits from the work will be:
Energy and Carbon footprint
Feedback control from electromagnetic sensors installed on strip run-out tables, continuous annealing production lines and heat treatment facilities will allow more efficient processing reducing overall energy consumption (e.g. reduced heat treatment times, reduced downgrading of product). Production of new AHSS steels to feed into the automotive industry will help towards lightweighting of the vehicle to meet the requirements of the Kyoto protocol and beyond.

Benefits to UK Industry and Society
The chief industrial beneficiaries are steel producers; Tata Steel employs approximately 11,000 people directly in the UK and produces 4 million tonnes of steel across several UK sites using controlled cooling strategies and heat treatment where microstructural information can be feedback into process control. EM sensing technology will allow efficient production of high value grades that are not currently commercially produced, which will increase the range of steel grades offered by the UK manufacturers. It should be noted that the ability to manufacture these value added steels will also increase sales of conventional steel grades, as customers often choose suppliers that can provide complete order coverage. This will provide the UK steel industry with a competitive advantage in the international market.
A secondary beneficiary will be sensor and mill control manufacturers. The EMspecTM system was developed at Primetals Technology Limited, based in Bournemouth, in collaboration with the University of Manchester following research carried out through previous EPSRC funded programmes. The development of fundamental magnetic property-microstructure relationships in this project will increase the accuracy of signal interpretations and potentially allow for integrated systems for control of cooling via dynamic feedback. Future exploitation of any new technology developed in this work will follow the established processes at Manchester and Warwick Universities as appropriate.
A further beneficiary of this project will be the automotive industry, which will have access to a UK source for AHSS products that can be used to lightweight vehicles. The automotive sector in the UK comprises over 3000 separate companies employing over 180,000 people. The UK has the sector's 4th highest output in Europe and the 12th highest globally. The use of new AHSS in automotive parts is vital to the competitive advantage of UK car manufacturers since the EU has defined legislation to meet the requirements of the Kyoto protocol and beyond.
Educational Impact
Within the project we are training four RFs. We will involve MSc and undergraduate students in the research area through offering related projects and two PhD students will be associated with the project. In addition exposure of younger students to the research area will be achieved via outreach activities (e.g. research fellows in the group are involved in school visits).

Publications

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Kahrobaee S (2022) Detection of Decarburising Depth in Hadfield Steels Using a Multi-magnetic NDE Method in Nondestructive Testing and Evaluation

 
Description A novel finite element microstructure model considering crystallographic texture (i.e. certain orientations of grains are preferred than the others) has been developed for predictting the anisotropic magnetic properties in ferromagnetic materials, e.g. ferritic steels. The model has proved to be capable of capturing the texture effect and the grain size effect and has been validated against grain-oriented electrical steel that has a strong texture.

The link between magnetic properties and key microstructural features in steels (phase balance, grain size) has been determined and modelled. The influence of temperature has also been considered. The development relationships have been used with EM sensor models to predict signals during transformation.
Exploitation Route The predicted magnetic properties, in particular, the effective magnetic permeability as a function of the measurement direction, can be used to predict the electromagnetic sensor (EM) signals for non-destructive testing. Together with the EM sensor model, the present microstructural model can serve as a promising modelling tool to look at anistropic materials properties in ferromagnetic materials including but not limited to steels. The data and modelling for the temperature-magnetic properties-microstructure relationships is being used for commercial (EMspec) sensor signal interpretation and the models are supporting industrial installations of the commercial sensor.
Sectors Manufacturing, including Industrial Biotechology

 
Description This project has helped to develop new sensor-signal relationships for monitoring microstructure of steel both during hot processing and for non-destructive testing of samples at room temperature. The relationships between microstructure-magnetic properties-temperature have supported the interpretation of commercial sensor signals for the array of sensor installed at the Tata Steel IJmuiden hot strip mill. The commercial sensor system (EMspec) are produced by Primetals Technology Limited using licensed technology from Manchester University support / developed during collaborative EPSRC project ASAP with WMG (EP/K027956/1)
First Year Of Impact 2015
Sector Manufacturing, including Industrial Biotechology
Impact Types Economic

 
Description Manufacturing the Future Hub grant SUSTAIN
Amount £10,468,988 (GBP)
Funding ID EP/S018107/1 
Organisation Engineering and Physical Sciences Research Council (EPSRC) 
Sector Public
Country United Kingdom
Start 04/2019 
End 03/2026
 
Description Online Microstructural Analytics
Amount € 3,747,804 (EUR)
Funding ID 847296 - OMA - RFCS-2018 
Organisation Research Fund for Coal and Steel 
Sector Public
Country Belgium
Start 07/2019 
End 12/2022
 
Description SUSTAIN STEEL HUB ECR
Amount £55,834 (GBP)
Organisation Engineering and Physical Sciences Research Council (EPSRC) 
Sector Public
Country United Kingdom
Start 12/2020 
End 12/2021
 
Description Smart Steel Alloy Manufacturing
Amount £894,901 (GBP)
Funding ID 8286 
Organisation High Value Manufacturing Catapult 
Sector Private
Country United Kingdom
Start 09/2022 
End 03/2025
 
Description Transforming the Foundation Industries: a Network+ ECR call 2
Amount £30,000 (GBP)
Funding ID EP/V026402/1 
Organisation Engineering and Physical Sciences Research Council (EPSRC) 
Sector Public
Country United Kingdom
Start 06/2022 
End 12/2022
 
Description Collaboration with Zapp on feasibility study 
Organisation Zapp Precision Metals
Country Germany 
Sector Private 
PI Contribution Discussed potential techniques to improve the non-destructive evaluation of their products including stainless steel wires. We have started initial feasibility studies to look at the magnetic domains of some of their products.
Collaborator Contribution Sent specimens for initial feasibility studies.
Impact Work is still ongoing
Start Year 2019
 
Description Invited talk and visit to Iwate University 
Form Of Engagement Activity A talk or presentation
Part Of Official Scheme? No
Geographic Reach Local
Primary Audience Professional Practitioners
Results and Impact Research Fellow, Dr Jun Liu, visited Professor Yasuhiro Kamada and Professor Satoru Kobayashi and gave a seminar. Jun visited their labs and discussed potential collaborations.
Year(s) Of Engagement Activity 2019
 
Description Invited talk at The 16th International Workshop on 1&2 Dimensional Magnetic Measurement and Testing - 2021 
Form Of Engagement Activity A talk or presentation
Part Of Official Scheme? No
Geographic Reach International
Primary Audience Professional Practitioners
Results and Impact Since its inception in Braunschweig in 1991, the 1&2DM conference series has brought together academic and industrial specialists in the field of magnetic measurement and testing and will provide opportunities to exchange the latest developments, ideas and experiences in the fields of magnetic measurement, magnetic testing and relevant modelling during technical and networking sessions.

1&2DM21 will consist of two days of talks and plenaries.

We gave a talk on the subject of real time EM sensor measurement for steel microstructures. I was well received with some questions from the audience. Some nice comments received and led to further discsussion.
Year(s) Of Engagement Activity 2021
URL https://2dm2021.com/
 
Description Invited talk at Transforming Foundation Industries Network+ ECR funding call 
Form Of Engagement Activity A talk or presentation
Part Of Official Scheme? No
Geographic Reach National
Primary Audience Professional Practitioners
Results and Impact The Transforming Foundation Industries Network+ has available funding for small projects of between 3 and 6 months duration. The TFIN+ is keen to attract applicants who are currently Post-Doctoral Researchers and who may wish to explore ideas that may have a transformative impact on the foundation industries (glass, metals, cements, ceramics, paper and bulk chemicals).

Frank Zhou gave a talk sharing experience on early career researchers apply for a small funding. How low TRL level research can benefit the Foundation Industries
Year(s) Of Engagement Activity 2022
URL https://www.eventbrite.co.uk/e/tfin-workshop-for-post-doctoral-researchers-funding-for-small-project...
 
Description Iommm conference attendance 
Form Of Engagement Activity A talk or presentation
Part Of Official Scheme? No
Geographic Reach International
Primary Audience Industry/Business
Results and Impact More than 62 delegates from Europeans countries and USA attended the IOMMM '' In-line measurement and control for metals'' conference 2017 hosted at University of Warwick.
Year(s) Of Engagement Activity 2017
URL https://www.iom3online.org/iom/frontend/reg/tOtherPage.csp?pageID=365196&eventID=731&msID=1734&pd=70...
 
Description Keynote Presentation 2nd International Conference on Applied Science and Aerospace Engineering 
Form Of Engagement Activity A talk or presentation
Part Of Official Scheme? No
Geographic Reach International
Primary Audience Professional Practitioners
Results and Impact Research Fellow, Dr Jun Liu, presented his latest work on the conference.
Year(s) Of Engagement Activity 2019