3D in-situ based methodology for optimizing the mechanical performance of selective laser melted aluminium alloys

Lead Research Organisation: University of Aberdeen
Department Name: Engineering

Abstract

Additive Manufacturing (AM), also known as 3D printing, is a common term used to describe the technology in which three-dimensional (3D) objects are fabricated by successive layers of material. The UK has been at the forefront of global innovation in AM and has also set up applications for commercialisation of this technology. While AM has been commonly employed for producing prototypes and tooling for decades, UK manufacturing industry has more recently been making revolution by using this technology for end-use products in various key sectors due to its economic and technical benefits in comparison with traditional manufacturing techniques. Once the current barrier to adoption of AM (i.e., quality, uncertainty of the final component and expertise) has been addressed, it is expected that this new emerging time-efficient AM technology has obvious capability to considerably boost UK economic production.

Selective laser melting (SLM) is one of the most promising metal AM methods where 3D components are fabricated by using a high-energy laser beam to fuse the pre-deposited metal powder. The use of SLM has been progressively increasing in a number of UK industrial sectors (i.e., aerospace, automotive, medical, oil & gas, marine and defence etc.) owing to its capability to produce near-net shape complex components from a CAD model and hence offering robust design flexibility without the constraints of conventional manufacturing methods that require a series of manufacturing processes, more material consumption, higher cost and energy. For manufacturing industry that targets to fabricate their products rapidly and access to wider purchaser markets, SLM appears to be an ideal route for their businesses if the inter-related relationships between process parameters and their ultimate effect on the structural integrity and performance has been established.

SLM is prevalently used to build in a range of metallic materials including stainless steel, titanium, nickel and aluminium alloys. Unlike the other alloys, manufacturing aluminium alloys by SLM involves more complexities due to being their high reflectivity and thermal conductivity which contribute to stimulate porosity in manufactured parts. Hence, there is presently a lack of understanding about the effect of SLM process parameters on microstructure and material performance in aluminium alloys. Determining such unknown relationships are an essentially important engineering mission that presently represents a major barrier to widespread usage of SLM processed aluminium alloys.

The overall aim of this First Grant proposal is to develop a robust methodology to optimize the manufacture of aluminium alloy components using selective laser melting. In achieving this, the combined use of X-ray microcomputed tomography with an in-situ microtensile testing stage (allowing observations of the 3D in-situ deformation) will be employed to investigate the impact of process parameters on porosity, material properties and failure behaviour. In addition, an experimentally based porous plasticity finite element model will be developed to understand the effect of void size and shape on deformation behaviour.

Planned Impact

This project will provide a method to optimize the manufacture of aluminium alloy components produced using selective laser melting (SLM), a metal additive manufacturing (3D printing) method. The possible benefits of this research proposal to society beyond the academic world is projected to be high as the methodology developed in this study can be widened to include a range of additive manufactured metallic materials such as steel, titanium and nickel alloys.

There having been continuous investment and innovation in producing SLMed parts by companies and the UK funding agencies, the use of SLM of aluminium alloys (similar to the other SLMed materials) has been progressively increasing in a number of UK industrial sectors. The outcomes of the research will assist UK and worldwide organizations in adopting SLMed aluminium alloys for next generation designs.

Particular benefits will be to: better understand the impact of process parameters on mechanical performance and quality assurance; determine limits for acceptable void sizes and shapes for designs; obtain key material properties to be standardized; provide a better understating of the effect of residual stresses on the material properties; lower development cost and time, gain confidence in design and reduce material wastage. The more widespread uses of SLM will allow decreases in carbon dioxide footprint associated with manufacturing.

The proposal has been developed based on series of discussions with the collaborators (e.g., Lloyd's Register (LR), The Welding Institute (TWI)) and project partners (the Advanced Materials & Processing Laboratory (AMPLab) at the University of Birmingham, the Manufacturing Technology Centre (MTC) and the Los Alamos National Lab (LANL)), certifying that directions of the proposed work will address their issues. The MTC and AMPLab will benefit from the outcomes of the project by correlating the process parameters with the volumetric defect formation and their effect on failure. The experimental results obtained will provide a detailed database for the LANL researchers working in additive manufacturing.

Potential wider beneficiaries in the UK and worldwide working with SLM will be sought through the existing collaborators and partners. Arranged meetings and discussions with industrialists and policy-makers by means of the MTC will enable the outcomes of the project to be exploited broadly. Any datasets produced in this project will be made available to other researchers via PURE which is the university's repository used to comply with EPSRC requirements. A budget for data storage is allocated and the presence of such data will be publicized through the project website, conference disseminations and Dr Kartal's social media accounts (i.e. LinkedIn and ResearchGate). This will help wider beneficiaries to accesses data obtained from projects.

This project will train a PDRA to develop transferable skills in materials modelling, characterization and testing which can be applied to a broad range of materials.
 
Description Internal porosity of metallic parts manufactured by 3D Metal Printing (3DMP) is governed by processing parameters including laser power, scanning speed, scan spacing and layer thickness. In work package 1 (WP1), to fully understand the influence of processing parameters, we have categorized the shape of process defects (pores) in 3D. AlSi10Mg samples were manufactured using 30 unique 3DMP parameter combinations and analysed using high resolution X-ray micro computed tomography (XµCT). The shapes of individual pores were classified and studied using an approach based on the similarity of 3D pore descriptors with simplified artificial objects. Porosity within high as-fabricated densification builds can be reduced to virtually negligible by hot isostatic pressing (HIPping), which was found to fully or partially close (flatten) pores. Subsequent T6 treatment causes pores to reopen and resemble their original shape. The effects of treatment are sensitive to pore size.

In work package 2 (WP2), the impact of pores caused by processing parameters on failure mechanisms have been investigated. A combination of XµCT and an in-situ micro-testing stage was employed to acquire 3D pictures at different loading stages. Specimens were tested in the as-built condition and following hot isostatic pressing (HIPping) or HIPping with T6. Process conditions (as-built, HIP and HIP+T6) have shown a significant impact on 3D pore evolution within AlSi10Mg. Under tensile deformation, voids in the as-built condition do not change markedly while the most substantial change occurs in the HIPped material. The technique used in WP2 provides us with deformation measured by a cross-head of the in-situ machine. Obviously such displacement involves the combination of actual deformation of the sample and compliance of the machine. The latter one is not due to actual deformation and hence it should be removed from the total displacement. In order to accurately measure deformation, a there dimensional algorithm has been developed in order to measure deformation of the samples by comparing images at different stages of loading.
Exploitation Route The approach outlined in this work can be used to study the influence of other processing parameters not investigated here for brevity and can equally be applied to study other 3DMP alloys. The approach outlined in WP2 can be used to investigate the evolution of pores of different size, shape and orientation within AlSi10Mg and other alloys processed using varying SLM parameters and build conditions. The developed algorithm is general and hence can be applied to different samples.
Sectors Aerospace, Defence and Marine,Manufacturing, including Industrial Biotechology

 
Description Findings have been shared with audiences in a conference proceeding Alloys for Additive Manufacturing Symposium 2019, Gothenburg, Sweden. A 4th year undergraduate project student studied 3D metal printing; and reproduced and expanded findings. She got first class honour mark for her individual project. The principal investigator has started teaching a short lecture on 3D metal printing for undergraduate 3rd year mechanical engineering students. Findings in the project help student visualize and better understand the topic. In order to maximize dissemination and use licensed materials, a journal paper has been very recently published in an open access journal (Materials and Design) with CC BY Gold Open license. An EPSRC sponsored workshop has been carried out on 10 March 2021. Due to Covid19, the workshop was purely online. Many researchers and people from industry participated in the meeting and the results of this project have been disseminated to audiences. In addition, researchers presented their own results. The workshop was informative.
Sector Education
 
Description Moataz Attallah 
Organisation University of Birmingham
Department School of Metallurgy and Materials
Country United Kingdom 
Sector Academic/University 
PI Contribution The partner benefited from the outcomes of the project by correlating the process parameters with the volumetric defect formation and their effect on failure.
Collaborator Contribution The samples used in this project have been manufactured in Advanced Materials and Processing Laboratory (AMPLab) at the University of Birmingham. The partner also supplies the investigator with their experience in the field and very useful guidance on selective laser melting.
Impact Hastie, JC, Kartal, M, Carter, LN, Attallah, MM & Mulvihill, DM 2020, 'Classifying shape of internal pores within AlSi10Mg alloy manufactured by laser powder bed fusion using 3D X-ray micro computed tomography: influence of processing parameters and heat treatment', Materials Characterization, vol. 163, 110225. Hastie, JC, Kartal, ME, Attallah, MM & Carter, LN 2019, 'Analysing size and shape of internal processing defects within selective laser melted aluminium alloy using x-ray micro computed tomography', Alloys for Additive Manufacturing Symposium 2019, Gothenburg, Sweden, 18/09/19 - 20/09/19 pp. 49-49.
Start Year 2018