Responsive Manufacturing of High Value Thin to Thick Films.

Lead Research Organisation: University of Sheffield
Department Name: Chemical & Biological Engineering

Abstract

Thin films with a high technical specification are used in many everyday devices, including displays, solar cells, electronic devices, batteries, and sensors. Printing of the high-value flexible electronic films with insulating, dielectric, semiconducting and conducting materials used in these devices makes a major and rapidly growing contribution to UK industry.The thickness of the films required, the starting materials used and the final high-value functions desired in the finished product vary significantly. However, the scientific principles that govern the behaviour of the printing processes for these diverse applications have many similarities, because they are all formed by selectively spreading a wet film of suspended solid particles and drying it.

At present the optimisation of the printing parameters for these films is commonly achieved through a trial and error process rather than systematic intelligent control. Individual processes are being optimised in isolation without cross-fertilization of knowledge. In a fast changing world, where disruption to supply chains or development of improved materials can change the process input materials, the need to reconfigure the formulations/printing parameters used increases. Furthermore, desired outputs can also change rapidly as the manufacturers and customers seek to meet changing demands of their market for example requiring more precise control of film parameters such as thickness and electrical properties. Adjusting to such continually moving goal posts by relying on trial and error testing is time-consuming, wasteful and costly.

The responsive manufacturing technology we propose to develop will have sufficient flexibility to overcome such problems by utilizing intelligent machine learning to control the printing parameters in real-time and therefore maintain an optimized printing process robustly in the face of variations in feedstock materials and/or the required output. It is surprising that there has been no major attempt to implement this approach to process control and optimisation for solution printed materials. This is despite process monitoring and feedback-based optimisation being proven enabling methods in other sectors such as additive manufacturing.

This will be achieved by developing control algorithms for the printing process that take into account our theoretical understanding of the processes occurring and utilizing high-speed (minimized and proxy) in situ data acquisition to respond autonomously and continuously to perturbations in the feedstock materials or required film properties. We will make use of the wide range of laboratory scale processing systems our project team regularly use for the production of model colloidal films, ceramic dielectrics, photovoltaics and battery electrodes to provide the datasets required to educate the machine learning algorithms, test our theoretical understanding, develop models of the printing processes and to ultimately test the autonomous control system that we develop. Having proven the system works at a laboratory scale we plan to perform a series of demonstration runs at industrial scale in collaboration with project partners CPI who are world leading experts in production of printed electronics. This will provide the evidence needed to prove that this approach can work at an industrial scale in a highly demanding production environment (printed electronics require a high degree of control of the surface chemistry between subsequent layers to perform correctly and are typically made in cleanroom/glove-boxes within strict environmental tolerances). We envisage a future where a deep theoretical understanding of the processes that are taking place is utilised by artificial intelligence to continuously control and optimise the manufacture of 21st century high-value printed films autonomously using the minimum number of high-speed measurements to achieve the desired results.

Publications

10 25 50
 
Description Attendance at the MACH 2022 Exhibition 
Form Of Engagement Activity A talk or presentation
Part Of Official Scheme? No
Geographic Reach National
Primary Audience Industry/Business
Results and Impact Attendance by project member and WP5 lead, Dr Hussam Muhamedsalih. Engaged with other attendees at the exhibition and promoted the work of the group in his discussions.
Year(s) Of Engagement Activity 2022
URL https://www.machexhibition.com/
 
Description EPSRC Net Zero event 
Form Of Engagement Activity Participation in an activity, workshop or similar
Part Of Official Scheme? No
Geographic Reach National
Primary Audience Policymakers/politicians
Results and Impact Attendance by WP5 lead (Dr Hussam Muhamedsalih) and WP6 lead (Prof Rachael Rothman). This was an event related to the governments Net Zero event that was part of COP26 in Glasgow.
The event was a hybrid event so it is difficult to understand the audience and the reach. Both our attendees were there in person.
Dr Muhamedsalih was an invited attendee as an Early Career Researcher and he provided a video that was relevant to the project and lead discussions afterwards.
Prof. Rothman attended as WP6 lead which relates to sustainability so talked with industry and government officials about the project.
Year(s) Of Engagement Activity 2022
URL https://www.ukri.org/events/epsrc-engineering-net-zero-showcase/
 
Description EPSRC Responsive Manufacturing meeting 
Form Of Engagement Activity A formal working group, expert panel or dialogue
Part Of Official Scheme? No
Geographic Reach National
Primary Audience Professional Practitioners
Results and Impact Prof Howse was invited to attend a meeting of other EPSRC funded academics who had been awarded similar responsive manufacturing grants. This was an opportunity to network and make connections with people of a similar research background. This will become an ongoing meeting following this first meeting.
Year(s) Of Engagement Activity 2022
 
Description New Trends in Metrology, Lublin University of Technology and the Central Office of Weights and Measures 
Form Of Engagement Activity Participation in an activity, workshop or similar
Part Of Official Scheme? No
Geographic Reach International
Primary Audience Industry/Business
Results and Impact WP3 lead Dr Liam Blunt alongside Dr Hussam Mohamedsalih and Dr Mothana Hassan presented to an audience of industry and academics, including work that is relevant to this project.
Year(s) Of Engagement Activity 2022
URL https://polishscience.pl/en/international-metrology-conference-new-trends-in-metrology-held-in-lubli...
 
Description SPIE (Smart Structures & Nondestructive Evaluation) CA, USA 
Form Of Engagement Activity A talk or presentation
Part Of Official Scheme? No
Geographic Reach International
Primary Audience Industry/Business
Results and Impact WP3 lead (Dr Liam Blunt) and WP5 lead (Dr Hussam Muhamedsalih) were invited to provide an abstract and to be invited speakers at this event in Long Island, California.
Year(s) Of Engagement Activity 2022
URL https://spie.org/conferences-and-exhibitions/smart-structures-nde?SSO=1