Electron Microscopy of Advanced Materials

Lead Research Organisation: University of St Andrews
Department Name: Chemistry

Abstract

The electron microscopy laboratory at University of St Andrews, equipped with a JEOL JEM-2011 transmission electron microscope (TEM) and a JEOL JSM-5600 scanning electron microscope (SEM), was established in 1999 and has been furnished with major accessories including a MacTempas Image Simulation System, a Gatan 656 Dimple Grinder, a Gatan 691 Precision Ion Polishing System and a fully equipped darkroom. Both TEM and SEM have an Oxford Instruments energy-dispersive X-ray spectrometer. TEM images are normally recorded with a Gatan CCD camera and can be transferred to user's own computer through the university network. This laboratory will open for external users of UK academic institutions and industry in order to optimise the use of the equipment and to enhance the collaboration between researchers in different universities.One day per week for each microscope will be reserved for external users and the availability of the service will be marketed on the school website. The process of the service and arrangement of materials research projects will be monitored by an Advisory Committee led by the Vice Principal for Research, Professor Alan Miller with other members from several universities. Lecture course on electron microscopy and one-to-one training course can be offered under requirement.

Publications

10 25 50

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Alharthi A (2014) Iron ochre - a pre-catalyst for the cracking of methane. in Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)

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Geng J (2008) Crystal structure and growth mechanism of unusually long fullerene (C60) nanowires. in Journal of the American Chemical Society

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Greer H (2011) Early stages of non-classic crystal growth in Science China Chemistry

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Greer H (2012) Hidden crystalline components in mesoporous silicate in Journal of Materials Chemistry

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Greer H (2016) Synthesis and Formation Mechanism of Textured MOF-5 in Crystal Growth & Design

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Hill A (2011) Neutron powder diffraction and magnetic studies of mesoporous Co3O4 in Journal of Magnetism and Magnetic Materials

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Huang WY (2013) Nanosegregation and neighbor-cation control of photoluminescence in carbidonitridosilicate phosphors. in Angewandte Chemie (International ed. in English)

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Jin X (2007) Nanoscale microelectrochemical cells on carbon nanotubes. in Small (Weinheim an der Bergstrasse, Germany)

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Self K (2016) Surface Charge Driven Growth of Eight-Branched Cu 2 O Crystals in Crystal Growth & Design

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Self K (2015) Reversed Crystal Growth of RHO Zeolitic Imidazolate Framework (ZIF). in Chemistry (Weinheim an der Bergstrasse, Germany)

 
Description This service centre has been used by more than 100 researchers from more than 20 UK universities. Some joined publications are listed (not completed because many papers were published by the users).
Exploitation Route The services offered to the UK university users have certainly strengthened their research in solid state chemistry and materials science. The training of electron microscope users led to more than 20 independent operators.
Sectors Chemicals,Energy,Environment

 
Description This program offers free access to the electron microscopes at St Andrews. A large number of UK university researchers have been benefited. It is the most economic way to share large research facilities. Collaboration between groups and universities have been encouraged and a healthy research atmosphere was created. Almost all the users sent positive comments on the service and wished to see possible continuance of the project.
First Year Of Impact 2007
Sector Chemicals,Energy,Environment
Impact Types Societal,Economic,Policy & public services