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Ultrafast Scanning Thermal Microscope Probes

Lead Research Organisation: University of Glasgow
Department Name: School of Engineering

Abstract

Heat is a universal quantity. Since all energy turns to heat, the study of thermal phenomena is applicable over the whole range of science and engineering. For example, the performance of many modern semiconductor devices are limited by their thermal performance e.g. RF power transistors, lasers, power switches and microprocessors. At the macroscopic scale thermal effects are generally slow, because heat transport is diffusive. A characteristic of diffusive phenomena is that they speed up quadratically with changes in dimension: If a device or thermometer is made ten times smaller it will have a thermal response which is a hundred times faster. In a normal material the effects can become enormously rapid, in the GHz range for modern devices which is a rate with is comparable to their operating frequency.

At the nanometre scale, where modern devices and materials are fabricated, the transport of heat ceases to be classical and diffusive. Heat may travel "ballistically" without scattering across a small distance leading to even more rapid thermal transport in a small device and the thermal conductivity of narrow wires may be quantised by the dimensions of the thermal conductor so that classical values of thermal conductivity do not apply and prediction of the thermal performance of such systems becomes impossible: it can only be measured. Since heat is often transported by sound waves known as transverse acoustic phonons which may have a wavelength which approaches the atomic spacing in the material the influence of interfaces between materials and their roughness on the atomic scale has a huge effect on how well structured materials may conduct heat. This might be used to advantage in thermoelectric materials or thermally insulating materials, or it may be an enormous problem when trying to extract the heat of operation from a device such as a laser or microprocessor. Again, since the technological control of atomic scale interfaces is hard this makes thermal conduction across interfaces impossible to predict, so we are forced to measure it.

Scanning Thermal Microscopy is a technique using the mechanical scanning of a sensor probe over a surface to make measurements of local temperature at the nanometre scale. This is very effective but currently the sensors used are very slow in response time, because they are relatively large (about ten micrometres) and are supported by large volumes of thermally insulating material. This project is concerned with the complete re-engineering of the probe to make it much smaller and to fabricate it without the use of thick support structures. This will allow the sensor to respond rapidly to the temperature variation of the sample and permit thermal measurements with a resolution of 30nm x 30nm x 1ns in the spatial and temporal domains.

The importance of such a probe is that it will, for the first time, enable the measurement of local temperature rise in devices and materials on the scale of device operation. Crucially, this will allow us to distinguish between heat being conducted away and heat being locally "stored" by heat capacity. This information allows the path of flow of heat to be determined through a device, enabling the designer to control it, and also determines the maximum temperature achieved. Since the thermal degradation of devices is limited by "thermal activation energy" the rate of damage and hence the lifetime of a device varies exponentially with temperature: The device lifetime is determined by the peak temperature, not the average. Since the properties of a material do not scale simply with size, and since the operating frequency of devices is fixed by device size, thermal measurements of the peak temperature can only be made at the spatial and temporal scales of the actual device. The proposed tools uniquely fulfil this requirement for measurements at the very heart of modern technological achievements.

Publications

10 25 50
 
Description The research was concerned with the development of "ultrafast scanning thermal microscope probes". Scanning thermal microscope probes are the essential sensor used to measure thermal phenomena at the nanoscale using a scanning thermal microscope. The probes incorporate a small resistance thermometer on a cantilever used in an atomic force microscope. Normally these sensors are about 10 µm long which limits the time taken to heat and cool down, limiting the speed to about 1kHz. The probes developed in this project were much smaller (down to 200nm long). Since the response rate of the probes is limited by thermal diffusion the speed improves as the square of the dimensional change, giving the new probes a predicted speed of 2.5 MHz. The probes were fabricated on high resistivity silicon (new) and integrated with a coplanar waveguide feed permitting efficient coupling to high frequency measurement systems (new). This waveguide technology is currently being tested by the University of Lille for potential use in scanning microwave microscopy. The probes were successfully fabricated and fully functional. The probes are the key enabling technology for high speed thermal microscopy. They will, for the first time, allow access both to the thermal conduction of materials at the nanoscale and also to the thermal diffusion (and hence heat capacity). The status of the project is that the instrumentation to apply the probes is being developed. Although this is itself a challenging task, it is essentially a well constrained technical challenge, rather than a speculative leap forward (like the probes themselves). Following this, the next stage is a new and similarly transformative problem of the development of a brand new experimental methodology to make use of the probes in the context of a quantitative and (to the extent that it is meaningful) traceable measurement. Funding for this aspect of the work has been applied for under the EPSRC instrumentation programme as a responsive mode grant application APP32042.
Exploitation Route The funding has enabled a fundamental change of the nature of thermal measurement technology at the nanoscale. Heat flow is determined by conduction, convection and radiation (static) and heat capacity (dynamic). The nature of thermal transport at the nanoscale is fundamentally different to that in macroscopic objects. Heat is transported by different carriers which may not be in mutual equilibrium. Transport of heat may be ballistic, causing a significant difference in temperature than that predicted by diffusive transport at longer length scales. Interfaces reflect phonons causing a dimensionless thermal impedance. The wavelength of acoustic phonons is comparable to the lattice spacing at room temperature in many important solids such as semiconductors. Thus the thermal impedance of an interface is large and depends on the atomic scale roughness of the interface, which is generally a poorly controlled technological parameter. For all these reasons (and especially the last) thermal measurement at the significant length scale (pretty much all modern devices are nano-scale in some dimension) is essential because the transport is not susceptible to a priori modelling or extrapolation from bulk measurements. Modelling *may* be useful but only after experimental calibration of the technological materials and structures using nanoscale measurement.
Sectors Aerospace

Defence and Marine

Digital/Communication/Information Technologies (including Software)

Electronics

Energy

 
Title SMM probe 
Description A monolithic scanning microwave microscope - AFM probe utilising a CPW feed to the probe tip, fabricated on high resistivity silicon and incorporating a force sensing cantilever. Provided to University of Lille for validation under EUROMET project "ELENA". Test as a SMM probe provides information on the waveguides used for ultrafast SThM probes 
Type Of Technology Systems, Materials & Instrumental Engineering 
Year Produced 2024 
Impact Awaited 
URL https://projects.lne.eu/jrp-elena/