Real-time In-line Microstructural Engineering (RIME)
Lead Research Organisation:
University of Warwick
Department Name: WMG
Abstract
Steel continues to be the most used material in the world by value and play an essential role in all aspects of society, from construction to transport, energy generation to food production. The long-term sustainability of UK steel making requires lower energy production and the development of high value steel products. The ability to measure the microstructure of steel in a non-contact, non-destructive fashion can lead to dramatic improvement in the understanding of the material and its behaviour during processing and in-service. Improved control during processing will increase efficiency in production of complex steel microstructures and allow new generation alloys to be made. Through our previous EPSRC and industry funded research we have created a new electromagnetic (EM) measurement system, EMspecTM, that can monitor the microstructure of strip steel during hot processing. This system is now providing information related to the condition (transformed phase fraction) of the microstructure over 100% of the strip length. The scene is now set to make the next major step forward with the information that new in-line microstructure measurement systems can offer - proposed real-time in-line microstructural engineering, or 'RIME' technology.
Our ambition is to enable real-time microstructure engineering during processing via dynamic control of cooling strategies or heat treatment using EM sensor feedback, in particular to engineer microstructures that were previously either impossible to achieve in full scale production or could not be reliably achieved. This will require detailed knowledge of the full temperature - magnetic - microstructure parameter space and sensors that are capable of operating in elevated temperature environments (such as heat treatment facilities), which are not currently available outside the laboratory. In addition application to a wide range of product lines, from strip to plate or sections requires integration of through thickness cooling models and EM signal-depth interpretation all mapped for varying temperature and phase fraction. In this project we will develop new sensors that can operate at high temperature; both laboratory systems to determine full magnetic properties with temperature for model and commercial steels, essential information that is currently unavailable in the literature, and robust deployable sensors for trials in industrial conditions; and systems designed to interrogate for through thickness data. We will develop a demonstration facility, consisting of a furnace, run out table with cooling sprays and EMspecTM system, to allow dynamic feedback control of cooling schedules from EM sensor signals to engineer specific microstructures. Alongside the hardware and demonstration activities we will also develop modelling capabilities, both for sensor design and signal interpretation: our current models are used to relate sensor signals to microstructure (phase fraction and grain size at room temperature) with incorporation of temperature effects planned in this project. A number of case studies have been identified to trial the new technologies including advanced high strength strip steels (AHSS) for light-weighting of vehicles, high strength - high toughness pipeline steels for demanding environments, high strength, more uniform, constructional steels and tailoring microstructure in rod.
Our ambition is to enable real-time microstructure engineering during processing via dynamic control of cooling strategies or heat treatment using EM sensor feedback, in particular to engineer microstructures that were previously either impossible to achieve in full scale production or could not be reliably achieved. This will require detailed knowledge of the full temperature - magnetic - microstructure parameter space and sensors that are capable of operating in elevated temperature environments (such as heat treatment facilities), which are not currently available outside the laboratory. In addition application to a wide range of product lines, from strip to plate or sections requires integration of through thickness cooling models and EM signal-depth interpretation all mapped for varying temperature and phase fraction. In this project we will develop new sensors that can operate at high temperature; both laboratory systems to determine full magnetic properties with temperature for model and commercial steels, essential information that is currently unavailable in the literature, and robust deployable sensors for trials in industrial conditions; and systems designed to interrogate for through thickness data. We will develop a demonstration facility, consisting of a furnace, run out table with cooling sprays and EMspecTM system, to allow dynamic feedback control of cooling schedules from EM sensor signals to engineer specific microstructures. Alongside the hardware and demonstration activities we will also develop modelling capabilities, both for sensor design and signal interpretation: our current models are used to relate sensor signals to microstructure (phase fraction and grain size at room temperature) with incorporation of temperature effects planned in this project. A number of case studies have been identified to trial the new technologies including advanced high strength strip steels (AHSS) for light-weighting of vehicles, high strength - high toughness pipeline steels for demanding environments, high strength, more uniform, constructional steels and tailoring microstructure in rod.
Planned Impact
This project aims to develop electromagnetic sensing technology to allow real-time in-line microstructural engineering for steels to give increased efficiency processing and enable production of new advanced high strength strip (AHSS) steel grades. The main benefits from the work will be:
Energy and Carbon footprint
Feedback control from electromagnetic sensors installed on strip run-out tables, continuous annealing production lines and heat treatment facilities will allow more efficient processing reducing overall energy consumption (e.g. reduced heat treatment times, reduced downgrading of product). Production of new AHSS steels to feed into the automotive industry will help towards lightweighting of the vehicle to meet the requirements of the Kyoto protocol and beyond.
Benefits to UK Industry and Society
The chief industrial beneficiaries are steel producers; Tata Steel employs approximately 11,000 people directly in the UK and produces 4 million tonnes of steel across several UK sites using controlled cooling strategies and heat treatment where microstructural information can be feedback into process control. EM sensing technology will allow efficient production of high value grades that are not currently commercially produced, which will increase the range of steel grades offered by the UK manufacturers. It should be noted that the ability to manufacture these value added steels will also increase sales of conventional steel grades, as customers often choose suppliers that can provide complete order coverage. This will provide the UK steel industry with a competitive advantage in the international market.
A secondary beneficiary will be sensor and mill control manufacturers. The EMspecTM system was developed at Primetals Technology Limited, based in Bournemouth, in collaboration with the University of Manchester following research carried out through previous EPSRC funded programmes. The development of fundamental magnetic property-microstructure relationships in this project will increase the accuracy of signal interpretations and potentially allow for integrated systems for control of cooling via dynamic feedback. Future exploitation of any new technology developed in this work will follow the established processes at Manchester and Warwick Universities as appropriate.
A further beneficiary of this project will be the automotive industry, which will have access to a UK source for AHSS products that can be used to lightweight vehicles. The automotive sector in the UK comprises over 3000 separate companies employing over 180,000 people. The UK has the sector's 4th highest output in Europe and the 12th highest globally. The use of new AHSS in automotive parts is vital to the competitive advantage of UK car manufacturers since the EU has defined legislation to meet the requirements of the Kyoto protocol and beyond.
Educational Impact
Within the project we are training four RFs. We will involve MSc and undergraduate students in the research area through offering related projects and two PhD students will be associated with the project. In addition exposure of younger students to the research area will be achieved via outreach activities (e.g. research fellows in the group are involved in school visits).
Energy and Carbon footprint
Feedback control from electromagnetic sensors installed on strip run-out tables, continuous annealing production lines and heat treatment facilities will allow more efficient processing reducing overall energy consumption (e.g. reduced heat treatment times, reduced downgrading of product). Production of new AHSS steels to feed into the automotive industry will help towards lightweighting of the vehicle to meet the requirements of the Kyoto protocol and beyond.
Benefits to UK Industry and Society
The chief industrial beneficiaries are steel producers; Tata Steel employs approximately 11,000 people directly in the UK and produces 4 million tonnes of steel across several UK sites using controlled cooling strategies and heat treatment where microstructural information can be feedback into process control. EM sensing technology will allow efficient production of high value grades that are not currently commercially produced, which will increase the range of steel grades offered by the UK manufacturers. It should be noted that the ability to manufacture these value added steels will also increase sales of conventional steel grades, as customers often choose suppliers that can provide complete order coverage. This will provide the UK steel industry with a competitive advantage in the international market.
A secondary beneficiary will be sensor and mill control manufacturers. The EMspecTM system was developed at Primetals Technology Limited, based in Bournemouth, in collaboration with the University of Manchester following research carried out through previous EPSRC funded programmes. The development of fundamental magnetic property-microstructure relationships in this project will increase the accuracy of signal interpretations and potentially allow for integrated systems for control of cooling via dynamic feedback. Future exploitation of any new technology developed in this work will follow the established processes at Manchester and Warwick Universities as appropriate.
A further beneficiary of this project will be the automotive industry, which will have access to a UK source for AHSS products that can be used to lightweight vehicles. The automotive sector in the UK comprises over 3000 separate companies employing over 180,000 people. The UK has the sector's 4th highest output in Europe and the 12th highest globally. The use of new AHSS in automotive parts is vital to the competitive advantage of UK car manufacturers since the EU has defined legislation to meet the requirements of the Kyoto protocol and beyond.
Educational Impact
Within the project we are training four RFs. We will involve MSc and undergraduate students in the research area through offering related projects and two PhD students will be associated with the project. In addition exposure of younger students to the research area will be achieved via outreach activities (e.g. research fellows in the group are involved in school visits).
Organisations
- University of Warwick (Lead Research Organisation)
- Zapp Precision Metals (Collaboration)
- Primetals Technologies (United Kingdom) (Project Partner)
- British Steel (United Kingdom) (Project Partner)
- Tata Group UK (Project Partner)
- Tenaris (United States) (Project Partner)
- Sheffield Forgemasters Engineering Ltd (Project Partner)
Publications
Aghadavoudi Jolfaei M
(2023)
Non-destructive evaluation of magnetic anisotropy associated with crystallographic texture of interstitial free steels
in Journal of Magnetism and Magnetic Materials
Aghadavoudi-Jolfaei M
(2019)
Non-destructive measurement of microstructure and tensile strength in varying thickness commercial DP steel strip using an EM sensor
in Journal of Magnetism and Magnetic Materials
B.L. Jones
(2022)
Magnetic characterisation of Strain Ageing in Near Eutectoid Drawn Pearlitic Wire using an Electromagnetic (EM) Sensor
in Journal of Engineering Failure Analysis
J. Shen
(2017)
Real-time microstructure control using EMspecTM sensor
Jones B
(2022)
Magnetic characterisation of strain ageing in near eutectoid drawn pearlitic wire using an electromagnetic (EM) sensor
in Engineering Failure Analysis
Kahrobaee S
(2022)
Detection of Decarburising Depth in Hadfield Steels Using a Multi-magnetic NDE Method
in Nondestructive Testing and Evaluation
Liu J
(2019)
Magnetic characterisation of grain size and precipitate distribution by major and minor BH loop measurements
in Journal of Magnetism and Magnetic Materials
Description | A novel finite element microstructure model considering crystallographic texture (i.e. certain orientations of grains are preferred than the others) has been developed for predictting the anisotropic magnetic properties in ferromagnetic materials, e.g. ferritic steels. The model has proved to be capable of capturing the texture effect and the grain size effect and has been validated against grain-oriented electrical steel that has a strong texture. The link between magnetic properties and key microstructural features in steels (phase balance, grain size) has been determined and modelled. The influence of temperature has also been considered. The development relationships have been used with EM sensor models to predict signals during transformation. |
Exploitation Route | The predicted magnetic properties, in particular, the effective magnetic permeability as a function of the measurement direction, can be used to predict the electromagnetic sensor (EM) signals for non-destructive testing. Together with the EM sensor model, the present microstructural model can serve as a promising modelling tool to look at anistropic materials properties in ferromagnetic materials including but not limited to steels. The data and modelling for the temperature-magnetic properties-microstructure relationships is being used for commercial (EMspec) sensor signal interpretation and the models are supporting industrial installations of the commercial sensor. |
Sectors | Manufacturing including Industrial Biotechology |
Description | This project has helped to develop new sensor-signal relationships for monitoring microstructure of steel both during hot processing and for non-destructive testing of samples at room temperature. The relationships between microstructure-magnetic properties-temperature have supported the interpretation of commercial sensor signals for the array of sensor installed at the Tata Steel IJmuiden hot strip mill. Further sensors are being installed in Tata Steel Port Talbot hot strip mill (2023/2024). The commercial sensor system (EMspec) are produced by Primetals Technology Limited using licensed technology from Manchester University support / developed during collaborative EPSRC project ASAP with WMG (EP/K027956/1). A new sensor array system has been developed and will be trialed in the Liberty Steel narrow strip mill (expected 2024). |
First Year Of Impact | 2014 |
Sector | Manufacturing, including Industrial Biotechology |
Impact Types | Economic |
Description | Manufacturing the Future Hub grant SUSTAIN |
Amount | £10,468,988 (GBP) |
Funding ID | EP/S018107/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 03/2019 |
End | 03/2026 |
Description | Online Microstructural Analytics |
Amount | € 3,747,804 (EUR) |
Funding ID | 847296 - OMA - RFCS-2018 |
Organisation | Research Fund for Coal and Steel |
Sector | Public |
Country | Belgium |
Start | 06/2019 |
End | 12/2022 |
Description | SUSTAIN STEEL HUB ECR |
Amount | £55,834 (GBP) |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 12/2020 |
End | 12/2021 |
Description | Smart Steel Alloy Manufacturing |
Amount | £894,901 (GBP) |
Funding ID | 8286 |
Organisation | High Value Manufacturing Catapult |
Sector | Private |
Country | United Kingdom |
Start | 08/2022 |
End | 03/2025 |
Description | Transforming the Foundation Industries: a Network+ ECR call 2 |
Amount | £30,000 (GBP) |
Funding ID | EP/V026402/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 05/2022 |
End | 12/2022 |
Description | Collaboration with Zapp on feasibility study |
Organisation | Zapp Precision Metals |
Country | Germany |
Sector | Private |
PI Contribution | Discussed potential techniques to improve the non-destructive evaluation of their products including stainless steel wires. We have started initial feasibility studies to look at the magnetic domains of some of their products. |
Collaborator Contribution | Sent specimens for initial feasibility studies. |
Impact | Work is still ongoing |
Start Year | 2019 |
Description | 25th International Workshop on Electromagnetic Nondestructive Evaluation (ENDE'22) |
Form Of Engagement Activity | A talk or presentation |
Part Of Official Scheme? | No |
Geographic Reach | International |
Primary Audience | Professional Practitioners |
Results and Impact | Talk given by M. A. JOLFAEI Measurement and Modelling Magnetic Anisotropy due to Crystallographic Texture in Interstitial Free (IF) Steels," in 25th International Workshop on Electromagnetic Nondestructive Evaluation (ENDE'22) |
Year(s) Of Engagement Activity | 2022 |
Description | Invited talk and visit to Iwate University |
Form Of Engagement Activity | A talk or presentation |
Part Of Official Scheme? | No |
Geographic Reach | Local |
Primary Audience | Professional Practitioners |
Results and Impact | Research Fellow, Dr Jun Liu, visited Professor Yasuhiro Kamada and Professor Satoru Kobayashi and gave a seminar. Jun visited their labs and discussed potential collaborations. |
Year(s) Of Engagement Activity | 2019 |
Description | Invited talk at The 16th International Workshop on 1&2 Dimensional Magnetic Measurement and Testing - 2021 |
Form Of Engagement Activity | A talk or presentation |
Part Of Official Scheme? | No |
Geographic Reach | International |
Primary Audience | Professional Practitioners |
Results and Impact | Since its inception in Braunschweig in 1991, the 1&2DM conference series has brought together academic and industrial specialists in the field of magnetic measurement and testing and will provide opportunities to exchange the latest developments, ideas and experiences in the fields of magnetic measurement, magnetic testing and relevant modelling during technical and networking sessions. 1&2DM21 will consist of two days of talks and plenaries. We gave a talk on the subject of real time EM sensor measurement for steel microstructures. I was well received with some questions from the audience. Some nice comments received and led to further discsussion. |
Year(s) Of Engagement Activity | 2021 |
URL | https://2dm2021.com/ |
Description | Invited talk at Transforming Foundation Industries Network+ ECR funding call |
Form Of Engagement Activity | A talk or presentation |
Part Of Official Scheme? | No |
Geographic Reach | National |
Primary Audience | Professional Practitioners |
Results and Impact | The Transforming Foundation Industries Network+ has available funding for small projects of between 3 and 6 months duration. The TFIN+ is keen to attract applicants who are currently Post-Doctoral Researchers and who may wish to explore ideas that may have a transformative impact on the foundation industries (glass, metals, cements, ceramics, paper and bulk chemicals). Frank Zhou gave a talk sharing experience on early career researchers apply for a small funding. How low TRL level research can benefit the Foundation Industries |
Year(s) Of Engagement Activity | 2022 |
URL | https://www.eventbrite.co.uk/e/tfin-workshop-for-post-doctoral-researchers-funding-for-small-project... |
Description | Iommm conference attendance |
Form Of Engagement Activity | A talk or presentation |
Part Of Official Scheme? | No |
Geographic Reach | International |
Primary Audience | Industry/Business |
Results and Impact | More than 62 delegates from Europeans countries and USA attended the IOMMM '' In-line measurement and control for metals'' conference 2017 hosted at University of Warwick. |
Year(s) Of Engagement Activity | 2017 |
URL | https://www.iom3online.org/iom/frontend/reg/tOtherPage.csp?pageID=365196&eventID=731&msID=1734&pd=70... |
Description | Keynote Presentation 2nd International Conference on Applied Science and Aerospace Engineering |
Form Of Engagement Activity | A talk or presentation |
Part Of Official Scheme? | No |
Geographic Reach | International |
Primary Audience | Professional Practitioners |
Results and Impact | Research Fellow, Dr Jun Liu, presented his latest work on the conference. |
Year(s) Of Engagement Activity | 2019 |
Description | Talk at 13th European Conference on Non-Destructive Testing (ECNDT) |
Form Of Engagement Activity | A talk or presentation |
Part Of Official Scheme? | No |
Geographic Reach | International |
Primary Audience | Professional Practitioners |
Results and Impact | Dr M. Jolfaei, gave a talk "Modelling Crystallographic Texture Evaluation and Non-Destructive Measurement of Magnetic Anisotropy using an Electromagnetic Sensor in Interstitial Free (If) Steels" at ECNDT conference 2023 |
Year(s) Of Engagement Activity | 2022 |
Description | Talk at 13th European Conference on Non-Destructive Testing (ECNDT) |
Form Of Engagement Activity | A talk or presentation |
Part Of Official Scheme? | No |
Geographic Reach | International |
Primary Audience | Industry/Business |
Results and Impact | 13th European Conference on Non-Destructive Testing (ECNDT) from 3 to -7 of July 2023 in Lisbon, Portugal (ECNDT 2023*) | Vol. 1(1). Dr Fanfu Wu gave a talk and the title was ''In-situ microstructure monitoring during tempering of quenched AISI4340 steels using a high temperature electromagnetic sensor.'' |
Year(s) Of Engagement Activity | 2022 |