High performance Wide spectral range Nanoprobe (HiWiN)
Lead Research Organisation:
Lancaster University
Department Name: Physics
Abstract
We propose to manufacture and commission the 'High performance Wide spectral range Nanoprobe' (HiWiN) using the tunable FEL electromagnetic (EM) radiation source FELIX (EPSRC National Research Facility at Nijmegen, Netherlands). HiWiN will enable area selective nanoscale (20-50 nm) illumination and/or light detection with high power and high intensity MIR-through-THz FEL radiation. HiWiN merges superior power, time signature and ultra-broad spectral tunability of the FELIX source (3 to 150 um) with selective ultra-high efficiency (20-70%) illumination/detection at the nanoscale. HiWiN has the ability to effectively concentrate the moderate to high power, spectrally selected, FEL EM radiation into a nanoscale-sized spot. This enables investigation of a wide variety of light-matter interaction phenomena (chemical reactions, molecular dissociation, nonlinear response). The project is supported by 31 UK research groups from multiple departments in 12 UK universities and the National Physics Laboratory. It is implemented by the multi-institutional collaboration lead by Lancaster University that is renowned for the development of nanoscale characterisation instrumentation that is now commercially available. HiWiN will be unique and world leading with no comparable capabilities existing in the UK or worldwide.
In particular the areas of research advanced by HiWiN will be Quantum Technology and materials where HiWiN will be able to zoom into individual single quantum dots generating THz radiation, to develop digital physical fingerprints to avoid counterfeited medicines, to focus on the special states of materials including two-dimensional materials and topological insulators, and to investigate ultrafast carrier dynamics in RF and THz devices. This research directly contributes to EPSRC growth areas of "Materials for energy applications" and "RF and microwave devices". Another major HiWiN impact area is Catalysis, which is internationally recognised as a critical enabling technology. Power FELs are an essential technology in catalysis allowing spectroscopic observation and initiation of chemical transformations in catalytic processes in real time. The high spatial resolution of HiWiN will provide unprecedented detail on catalytic processes, achieving characterisation of single active catalytic sites, single nanoparticles and enabling new understanding of surface chemical processes and reaction intermediates.
In the biomedical sciences, FELs and HiWiN provide the high power and high throughput essential to obtain high quality near field data in the MIR and THz region and this is particularly useful in the study of biological systems, where the functions, such as cell signalling and metabolism which can be targets for pharmaceuticals, are often controlled by submicron surface structures. It will make possible the characterisation of individual bacteria and complex microbial communities; image and characterise nanoparticles relevant to cancer therapies and Alzheimer biochemistry, and to observe nanoscale changes in biomedical monitoring. The combination of high-quality nanoscale imaging with intense THz radiation will open a new window on a detection of diseases and hydration of the cornea, and the interaction of THz radiation with living cells. The biomedical science programme of HiWiN is well aligned with EPSRC's Healthy Nation Strategy and UKRI Roadmap (Biological and biomedical imaging capability). It addresses many of UKRI's priorities supported by the Global Challenges Research Fund and Technology Touching Life programme.
We expect HiWiN to become a major platform triggering research in the multiple application areas and stimulating new technological solution in advanced scientific instrumentation.
In particular the areas of research advanced by HiWiN will be Quantum Technology and materials where HiWiN will be able to zoom into individual single quantum dots generating THz radiation, to develop digital physical fingerprints to avoid counterfeited medicines, to focus on the special states of materials including two-dimensional materials and topological insulators, and to investigate ultrafast carrier dynamics in RF and THz devices. This research directly contributes to EPSRC growth areas of "Materials for energy applications" and "RF and microwave devices". Another major HiWiN impact area is Catalysis, which is internationally recognised as a critical enabling technology. Power FELs are an essential technology in catalysis allowing spectroscopic observation and initiation of chemical transformations in catalytic processes in real time. The high spatial resolution of HiWiN will provide unprecedented detail on catalytic processes, achieving characterisation of single active catalytic sites, single nanoparticles and enabling new understanding of surface chemical processes and reaction intermediates.
In the biomedical sciences, FELs and HiWiN provide the high power and high throughput essential to obtain high quality near field data in the MIR and THz region and this is particularly useful in the study of biological systems, where the functions, such as cell signalling and metabolism which can be targets for pharmaceuticals, are often controlled by submicron surface structures. It will make possible the characterisation of individual bacteria and complex microbial communities; image and characterise nanoparticles relevant to cancer therapies and Alzheimer biochemistry, and to observe nanoscale changes in biomedical monitoring. The combination of high-quality nanoscale imaging with intense THz radiation will open a new window on a detection of diseases and hydration of the cornea, and the interaction of THz radiation with living cells. The biomedical science programme of HiWiN is well aligned with EPSRC's Healthy Nation Strategy and UKRI Roadmap (Biological and biomedical imaging capability). It addresses many of UKRI's priorities supported by the Global Challenges Research Fund and Technology Touching Life programme.
We expect HiWiN to become a major platform triggering research in the multiple application areas and stimulating new technological solution in advanced scientific instrumentation.
Publications
Ahmad M
(2022)
Engineering Interfacial Effects in Electron and Phonon Transport of Sb 2 Te 3 /MoS 2 Multilayer for Thermoelectric ZT Above 2.0
in Advanced Functional Materials
Canetta A
(2023)
Quantifying the local mechanical properties of twisted double bilayer graphene.
in Nanoscale
Chen Y
(2024)
Nonequilibrium fast-lithiation of Li4Ti5O12 thin film anode for LIBs
in Communications Physics
Chen Y
(2023)
Nanoarchitecture factors of solid electrolyte interphase formation via 3D nano-rheology microscopy and surface force-distance spectroscopy.
in Nature communications
Chen Y
(2021)
Controlling Interfacial Reduction Kinetics and Suppressing Electrochemical Oscillations in Li 4 Ti 5 O 12 Thin-Film Anodes
in Advanced Functional Materials
Chen Y
(2024)
Operando nano-mapping of sodium-diglyme co-intercalation and SEI formation in sodium ion batteries' graphene anodes
in Applied Physics Reviews
Chen Y
(2024)
Inhibiting the current spikes within the channel layer of LiCoO2-based three-terminal synaptic transistors
in Applied Physics Reviews
Evangeli C
(2024)
Thermoelectric Limitations of Graphene Nanodevices at Ultrahigh Current Densities.
in ACS nano
Gonzalez-Munoz S
(2023)
Direct Measurements of Anisotropic Thermal Transport in ?-InSe Nanolayers via Cross-Sectional Scanning Thermal Microscopy
in Advanced Materials Interfaces
Jarvis SP
(2021)
Chemical shielding of H2O and HF encapsulated inside a C60 cage.
in Communications chemistry
| Title | Supplement information |
| Description | Supplement information for the main manuscript |
| Type Of Art | Image |
| Year Produced | 2024 |
| URL | https://aip.figshare.com/articles/figure/Supplement_information/25773186 |
| Description | We have implemented the approach to effectively explore effects of the infrared and THz radiation, on the microscale and nanoscale. We also implemented the real time spectroscopic measurements of the broadband light radiation that can provide information on the biological objects, organic molecules and new two-dimensional materials correlating it with the nanoscale features of the studied objects. |
| Exploitation Route | This is the work in progress at the moment, but some of the published results are being reproduced and cited by other groups. 10.22443/rms.mmc2023.361 |
| Sectors | Aerospace Defence and Marine Agriculture Food and Drink Chemicals Electronics Energy Healthcare Manufacturing including Industrial Biotechology Pharmaceuticals and Medical Biotechnology |
| URL | https://www.mmc-series.org.uk/abstract/2072-sub-wavelength-focusing-of-mid-ir-light-using-metaldiamondmetal-campanile-probe-for-ultra-broadband-spm.html |
| Description | The scientific instrument companies - Bruker LTD, and Neaspec are considering using the new technology in their instruments. Also Dutch Diamond Technologies considering joint IP development with a view of production of new probes. |
| First Year Of Impact | 2023 |
| Sector | Manufacturing, including Industrial Biotechology |
| Impact Types | Economic |
| Description | 3D mapping of energy materials |
| Amount | £6,000 (GBP) |
| Funding ID | DST/NBHF/2020/1 |
| Organisation | Lancaster University |
| Sector | Academic/University |
| Country | United Kingdom |
| Start | 09/2021 |
| End | 01/2022 |
| Description | NEXGENNA, Faraday Institution |
| Amount | £11,000,000 (GBP) |
| Funding ID | NEXGENNA |
| Organisation | Lancaster University |
| Sector | Academic/University |
| Country | United Kingdom |
| Start | 12/2019 |
| End | 04/2024 |
| Title | Novel methodology for nanoscale characterisation |
| Description | Novel platform for the measurements and characterisation of materials and devices with ~ 10-50 nm spatial resolution using a diamond based ultra-broadband tool. |
| Type Of Material | Improvements to research infrastructure |
| Year Produced | 2022 |
| Provided To Others? | Yes |
| Impact | IP created and being discussed with the potential users. |
| URL | https://hiwin-felix.org/ |
| Title | Supplementary Online Material |
| Description | Supplementary Online Material |
| Type Of Material | Database/Collection of data |
| Year Produced | 2024 |
| Provided To Others? | Yes |
| URL | https://aip.figshare.com/articles/dataset/Supplementary_Online_Material/27058219 |
| Description | 2D MIR photodectors |
| Organisation | University of Nottingham |
| Department | School of Physics and Astronomy |
| Country | United Kingdom |
| Sector | Academic/University |
| PI Contribution | The HiWiN instrument enabling micro and nanoscale MIR and THz testing was adapted for studies of advanced 2D materials photodectors. |
| Collaborator Contribution | University of Nottingham (Prof. Amalia Patane's group) has provided a set of 2D material photodetectors made of Graphen and graphene-2DM material heterostructure. |
| Impact | The studies were jointly performed in Lancaster using QCL source and at University of Radboud FELIX free electron laser (EPSRC Mid-Range facility), with joint publications at the research conferences reported (AFM-SPM Meeting, Durhame, 2024) and submitted (MMC 2024)and journal paper in preparation. |
| Start Year | 2023 |
| Description | Bruker measurement methodology collaboration. |
| Organisation | Bruker Corporation |
| Department | Bruker Nano |
| Country | Germany |
| Sector | Private |
| PI Contribution | Developing new approach to nanoscale measurements using MIR and THz radiation. |
| Collaborator Contribution | Combining the scanning probe and the optical measurements. |
| Impact | Novel measurement nanoscale instrumentation. |
| Start Year | 2021 |
| Description | HiWiN instrument |
| Organisation | Radboud University Nijmegen |
| Department | High Field Magnet Laboratory (HFML) |
| Country | Netherlands |
| Sector | Academic/University |
| PI Contribution | Adapting HiWiN instrument at FELIX facility to the new projects. |
| Collaborator Contribution | Helped to accomodate HiWiN instrument for the FELIX MIR - THz beam line. |
| Impact | The system was added to the facility and offered on the competitive basis with priority to UK users. |
| Start Year | 2024 |
| Description | TE materials development |
| Organisation | University of Delhi |
| Country | India |
| Sector | Academic/University |
| PI Contribution | Measurements of the thermal transport in thin films otherwise impossible by other means. |
| Collaborator Contribution | Production of new efficient materials and measurement of their structural properties. |
| Impact | Development of extremely efficient thermoelectrics based on 2D-3D materials combination. |
| Start Year | 2022 |
| Title | New broadband MIR -THz micro/nanoprobe |
| Description | The new probe has been developed jointky with Dutch Diamond Technologies and is available to HiWiN users. |
| Type Of Technology | New/Improved Technique/Technology |
| Year Produced | 2024 |
| Impact | It became possible to effectively concentrate the electromagnetic radiation in the MIR THz region ins a sub-wavelength area of 100 nm - 10 um. THis can be used as an entirely new platform for the investigation of material and phenomena with micro/nanoscale resolution. |
| URL | https://hiwin-felix.org/ |
