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Manufacturing the Future with Supercritical CO2 and Minimum Quantity Lubrication

Lead Research Organisation: University of Leeds
Department Name: Mechanical Engineering

Abstract

Currently the dominant approach for cooling and lubricating machining processes, such as drilling, milling and turning, is to use emulsion-based coolants (otherwise known as metalworking fluids) at high flow rates. There are many serious environmental, financial and health and safety reasons for reducing industry's reliance on emulsion coolants - an estimated 320,000 tonnes/year in the EU alone, up to 17% of total production costs, and over 1 million people are exposed regularly to the injurious effects of its additives which can cause skin irritation and even cancers. Serious environmental problems are also caused by the up to 30% of coolant that is lost in leaks and cleaning processes and which eventually ends up polluting rivers.

These issues have motivated extensive research efforts to identify more sustainable machining processes. There is growing and compelling evidence from preliminary studies that cryogenic machining with supercritical CO2 (scCO2) with small amounts of lubricant (Minimum Quantity Lubrication, MQL, referred to as scCO2+MQL machining) can provide a high-performing and more sustainable alternative. Current knowledge gaps in the relationships between key input and output variables, the reasons for variations in performance and concerns over the release of CO2, are preventing a major uptake of this technology by UK manufacturers.

This project aims to test the hypothesis that optimising combinations of CO2 with small amounts of the appropriate lubricant can provide reliable, step-change improvements in the performance and sustainability of machining operations. It will carry out a systematic investigation into the effect of scCO2+MQL on cutting forces, heat and tool wear mechanisms during machining of titanium, steels and composite stacks. It will develop: (a) advanced experimental methods in combination with full-scale machining trials to explore how lubrication and heat transfer affect machining performance; (b) lifecycle assessment and scavenging methods for sustainable re-use of CO2; (c) machine learning methods to predict the relationships between process inputs and outputs and (d) develop an effective and efficient optimisation methodology for balancing competing financial, performance and sustainability objectives in scCO2+MQL machining. These will deliver the knowledge, experimental and modelling methods and software tools that UK industry needs to exploit this enormous as-yet untapped potential.

The project will involves staff and postdoctoral research assistants from the Universities of Leeds and Sheffield and the Advanced Manufacturing Research Centres in Sheffield, with advice and guidance from a Project Steering Group comprised of leading international academic and industrial experts. Collectively, the team has the expertise in (a) manufacturing systems and tribology; (b) energy systems and lifecycle assessment; (c) fluid mechanics and heat transfer, and (d) machine learning and optimisation, needed to provide the 'how' and 'why' UK industry needs to reliably achieve or exceed the performance improvements seen in preliminary studies, namely doubling of tool life. We will work with our industrial and business sector collaborators to drive transformations in machining rate, process cost and accompanying safety, environmental and quality metrics for the benefit of the UK's defence, civil nuclear and medical manufacturing industries through the 2020s and beyond.
 
Description The research activity funded through this awarded project has allowed for a lab-level examination of the consumption of a supercritical CO2 plus minimum quantity lubrication (scCO2+MQL) delivery system. Annual emissions and running costs have been calculated/ estimated, showing that CO2 flowrates used in the literature to date carry a significant economic and global warming impact. Thus the use of lower CO2 flowrates is recommended going forward, to transition this promising cooling and lubrication technology into larger-scale industrial usage. Lower flowrates can be achieved via the selection of system pressure and system exit nozzles. Furthermore it has been shown that productivity can be increased in titanium milling, via the use of scCO2+MQL instead of liquid emulsion-based coolants. Cutting tool damage rates were lowered by using scCO2+MQL, allowing for an increase of surface speed.
Exploitation Route This research will be transitioned from readiness level 3 (lab-based trials) towards larger-scale industrial usage in mass production, via University of Sheffield AMRC collaborative projects jointly funded with industry.
Sectors Aerospace

Defence and Marine

Manufacturing

including Industrial Biotechology

Transport

 
Description This award is in close partnership with industry; the technical work is supporting continuing engagement with industry who we are providing detailed underpinning findings to. There is a growing interest in the approach as a result of this work. Ultimately this will address the productivity of industry.
First Year Of Impact 2024
Sector Aerospace, Defence and Marine,Manufacturing, including Industrial Biotechology
Impact Types Societal

Economic

 
Description BOC Limited 
Organisation Linde Group
Department BOC
Country United Kingdom 
Sector Private 
PI Contribution Steering board membership; setting direction and supporting dissemination of results.
Collaborator Contribution Steering board membership; setting direction and supporting dissemination of results.
Impact Meeting attendance; steering group attendance
Start Year 2023
 
Description Collaboration with Seco Tools 
Organisation SECO Tools
Country United Kingdom 
Sector Private 
PI Contribution Research findings from the ongoing project will be shared with Seco Tools
Collaborator Contribution Seco will provide materials for testing to support us developing phenological understanding.
Impact Industrial meetings and advice to steering team for project. Supply of materials.
Start Year 2022
 
Description Partnership with University of Sheffield - AMRC 
Organisation University of Sheffield
Department Advanced Manufacturing Research Centre (AMRC)
Country United Kingdom 
Sector Academic/University 
PI Contribution This partnership has resulted in the award of EP/W001950/1. The partnership is a two-way research project with sharing of staff, techniques and research findings.
Collaborator Contribution AMRC are uniquely placed to bring real-world data in machining applications using supercritical CO2 - they also bring a strong industrial consortium
Impact Presentation at he Advanced Cooling day, 2023. Industry steering group outcomes to launch project.
Start Year 2022
 
Description Advanced Cooling day meeting 
Form Of Engagement Activity A formal working group, expert panel or dialogue
Part Of Official Scheme? No
Geographic Reach International
Primary Audience Industry/Business
Results and Impact Initial meeting bringing together 8 partner organisations to outline research direction and report early findings.
Year(s) Of Engagement Activity 2022
 
Description Formal workshop presentation activity 
Form Of Engagement Activity A formal working group, expert panel or dialogue
Part Of Official Scheme? No
Geographic Reach International
Primary Audience Industry/Business
Results and Impact Presentation of project (x3 presentations given in meeting)
Year(s) Of Engagement Activity 2023
 
Description Industrial interest in the cleanliness of supercritical CO2 as a machining coolant and lubricant 
Form Of Engagement Activity Participation in an open day or visit at my research institution
Part Of Official Scheme? No
Geographic Reach International
Primary Audience Industry/Business
Results and Impact Two staff visited our organisation, from a manufacturer based in the USA. They work on global process improvements. They were interested to hear about the supercritical CO2 machining carried out in this project, in terms of the cleanliness of tools and cut materials after the machining process is complete. Follow-up video calls are expected to occur.
Year(s) Of Engagement Activity 2025
 
Description Lecture on the social, economic and environmental profile of supercritical CO2 plus minimum quantity lubrication, as a coolant and lubricant 
Form Of Engagement Activity A talk or presentation
Part Of Official Scheme? No
Geographic Reach National
Primary Audience Undergraduate students
Results and Impact In late 2024, undergraduate Engineering students at the University of Leeds were introduced to the concept of the triple bottom line for sustainability: social, economic and environmental categories. A guest lecture was delivered by University of Sheffield AMRC TMG's Dr Chris Taylor. The social, economic and environmental aspects of supercritical CO2 were compared against emulsion liquid coolants, when used to cool and lubricate machining processes. The method to calculate and compare annual costs and carbon emissions was explained.
Year(s) Of Engagement Activity 2024