Additive Manufacturing: driving the Steel Industry into the digital age (AM-Steel)

Lead Research Organisation: Liberty Powder Metals Ltd
Department Name: Research and development

Abstract

Steel is the backbone of modern society, serving as the foundation for many industries globally. The widespread growth of the steel industry is tied directly to the Industrial Revolution and since then this growth has not stopped; global crude steel production was 1.7 billion tonnes in 2017. Over the years both steel materials and the processes we use to make them have been researched and developed continuously, but a lack of government support for industry meant new investment in existing steel manufacturing infrastructure was limited. In recent decades huge amounts of steel, sold cheaper than we can make it in the UK, have flooded the market. This comes primarily from Europe and Asia. In order to compete in this key industry the UK has to shift its focus from large volumes of commodity material to smaller volumes of high value-added material, and to achieve this in both an environmentally and economically sustainable way. This has been accepted in the industry but low profit margins have meant there are no funds available to invest in large capital projects and enable transformation on the required scale with current technologies.

This ambitious project, AM-Steel, aims to start to address this challenge by providing the UK steel industry with the knowledge, technology and competitive advantage required to kick-start a transformation towards digital technologies - specifically additive manufacturing (AM). The AM process is currently used in high-tech and high-value industries including Aerospace and Medical, where the design freedom and high material utilisation makes the economic benefit easily seen, and is experiencing unprecedented revenue growth of 40% year-on-year for the past 5 years. With the maturing of this technology, AM has started to spread into a broader range industry sectors, where steel is the dominant material. It is projected that from 2020 steel will have the largest market share in the metal AM sector, overtaking Titanium, Nickel, and Aluminium alloys.

AM requires high quality metal alloy powders. There are less than ten steel alloys widely available as powders for AM, mostly stainless and tool steels, compared to the thousands of alloys available to traditional productions routes (such as casting or forging and subtractive machining). This project will use the wealth of metallurgical knowledge in the steel industry, advanced thermodynamic modelling, and world-leading characterisation facilities - all available in the UK - to create a range of bespoke steel alloy compositions tailored to realise the enhanced processability at lower cost for general engineering applications, by utilising the unique benefits of the AM process.

AM-Steel will establish AM technology capability in the UK steel industry; enabling the industry to produce high value-added powder materials for AM, improving the productivity of the industry's heritage assets using these technologies, and transforming the industry and its supply chain through digital manufacturing.

AM-Steel is strategically aligned with the Liberty GREENSTEEL policy: to serve local markets using local materials; produced using green, renewable long-term sources of power; re-invigorating the subsequent engineering supply chain and delivering innovative solutions that provide a competitive advantage to customers. AM-Steel will contribute greatly to Liberty's target to be carbon neutral by 2030.

Planned Impact

Success of this project would generate economic, environmental and societal benefits.

Metal powders and Additive Manufacturing (AM) technologies are disruptive in nature, have the potential to create new products and to replace some traditional steel and metal products. Use of powder metals to manufacture components will produce lighter weight products, using and wasting less materials, and reduce the steps in the manufacturing process and supply chain. A broad spectrum of high value manufacturing industries including Aerospace, Automotive, Energy and Medical are investing in AM technologies, which this project will impact.

Economic benefits:
- The new materials developed in AM-Steel will help to realise the potential of AM for general engineering applications, leading to a higher uptake of AM technology which in turn will help drive down the cost of machinery and material through economies of scale thus enabling further cost reduction in a virtuous circle.
- By conservative estimates the productivity at selected Liberty Steel plants alone could be improved by 1% through the repair technology developed for steel plant components by 2025, resulting in a £10m revenue increase and benefits along the steel supply chain.
- The solutions to be developed in this project are applicable to other asset-intensive sectors beyond steel, and the knowledge transfer to enable this will be achieved through the dissemination activities written into the Pathway to Impact. Liberty and project partners will disseminate information with industrial and academic bodies through cross-function and multi-industry conferences and technical papers, with the intention of accelerating the pace of development.
- It is expected that the additional revenue at Liberty Powder Metals from sales of new materials during the project will be £1m and increase to £5m/pa 5 years after the fellowship. Liberty's business plan, if enabled by this project, would increase high value product export (£20m by 2025).

Environmental benefits:
- The material yield from current AM processes is above 95%, as compared to existing manufacturing routes that in Aerospace are closer to 15%, so energy and emissions are saved throughout the supply chain from less mineral extraction and processing to reduced transportation.
- The overall supply chain is much shorter, with less processes that due to their scale also tend to be vertically integrated with the AM facility, greatly reducing the transportation energy consumption and linked emissions.
- Significant light-weighting of components can be achieved due to the high specific strength of steel, which in turn can generate significant reduction in energy consumption and emissions

Societal benefits:
- Education, Employment and Skills are central to supporting a diversified and high value economy with a skilled workforce, while increasing lifetime opportunities for young people and older workers which will help ensure a more inclusive economy. The training programme provided will upskill existing employee's in the steel industry and supply chain and expand the talent pool to fill new job opportunities created by the transformation to digital manufacture in the upcoming decade.
- The AM technology capability developed through this project will enable Liberty, the UK steel industry and the wider supply chain to invest in powder metal businesses. Liberty's investment plan alone would create 50 new jobs in the business and an estimated 185 in supply chain, an this number could be much higher as UK steel and other sectors increase their investment in AM. Being a high-tech industry, the jobs created (or indeed those upskilled and saved from the struggling steel industry) by the growth of the AM industry would be high value and better secured.

Publications

10 25 50
 
Description In the past two years of this Future Leaders Fellowship program, significant progress has been made in three areas:

1. Alloy development for additive manufacturing
There are strong demands on new alloys for additive manufacturing as currently only a few alloys are commercially available.
- Three new alloys (low alloyed steel, stainless steel, tool steel) has been developed and successfully processed into powder. Microstructure analysis, printing trials and mechanical testing of these alloys are currently on-going. One grade has already shown very promising properties and a new patent application is currently in preparation.
- Successful trials of producing high value metal powder using recycled materials, such as machining chips, obsolete parts, failed AM build parts. This will fully integrate our powder production activity into the circular economy and reduce powder cost. Several commercial orders have been received to toll atomising recycled materials.
- Additive manufacturing has stringent requirements on powder quality, although some requirements are not well understood, such as powder flowability. This work has found that clean powders produced by vacuum melting gas atomising system have poor flowability, due to cohesive force between powders, not powder morphology. Adding flow additives to powder has improved flowability. This finding has given customers confidence in our powder quality. Currently fine powder can not be used for additive manufacturing due poor flowability. Further work will carried to explore the potential of flow enhancement by flow additives. It is envisaged that with the help of flow additives, finer powder could be used for additive manufacturing. This will not only greatly improve the saleable powder yield for powder manufacturers but also has the potential to reduce powder cost for end users.

2. Powder production process improvement
As a new powder business, there are huge challenges to stabilise and improve our production process.
- In 2021 we have found impurities in powder produced from some (around 20-30%) melt batches which significantly reduce powder quality and make the powder un-saleable. Through this award, we have found that impurities are coming from slags in melts. solution has been proposed and implemented in the production process. Latest production record has indicated this issue has been solved.
- We have found that the life of refractories used for melting are significantly below expectation. Crucibles recommended by supplier can only last for 1 to 8 melts. This has led to significant increase in crucible consumption and more importantly production down time. It was found that the failure of crucibles is due to cracking and erosion during melting under vacuum. Working with supplier, we are able to increase the crucible life to 20 to 30 melts through selection of a suitable refractory material system.

3. Leadership development
- Achieved membership (MIMMM grade) from the Institute of Materials, Minerals & Mining (IOM3)
- Completed higher level management training course (45 hours ), Leadership and Management in the Engineering and Construction Sectors provided by Middlesbrough College
- Completed three technical training courses provided by Manufacturing Technology Centre (CU36 Coordination of Additive Manufacturing, 7 hours) and European Powder Metallurgy Association (CU27 Additive Manufacturing with Steel Feedstock, 21 hours; CU30 Additive Manufacturing with Nickel Feedstock, 7 hours)
- Participated in the Scaling the Edge training program provided by Innovate UK.
- Provided knowledge and skill training to Liberty Powder Metals employees in the area of powder metallurgy, including powder production methods, powder processing and handling, additive manufacturing, hot isostatic pressing and applications.
- Participated Rapid+TCT trade show in Detroit, USA
- Participated WorldPM2022 Congress & Exhibition
- Invited presentation and member of expert panel discussion at International Conference on Additive Manufacturing 2022 (ICAM2022) organised by ASTM
Exploitation Route The outcomes of this funding have already generated significant benefits to Liberty Powder Metals, especially in the area of productivity improvement. Liberty Powder Metals will continue to be the main business in our exploitation plan but it is expected in the following years, other businesses in the additive manufacturing supply chain will benefit from this work, especially in the area of alloy development.
Sectors Aerospace, Defence and Marine,Energy,Environment,Manufacturing, including Industrial Biotechology,Transport

 
Description Our findings in the powder production process improvement area has led to productivity at Liberty Powder Metals improved by over 50% and out-of-spec product rate reduced by over 30% in 2021. In 2022, we have developed new production process to enable us to produce 3 materials using recycled materials. In the alloy development area, a number of businesses have shown great interest. Orders with total value over £200k have received. It was estimated that around £1.5m savings/additional revenue are directly attributed to this award so far. This award provides an opportunity to introduce additive manufacturing technology into the UK steel industry. Through this award, training has been provided to Liberty Powder Metals operators and engineers to up-skill their knowledge and skill in this rapid growing new technology. In the following years, training will be provided to steelworkers in the wider UK steel industry and business in the AM supply chain.
First Year Of Impact 2021
Sector Aerospace, Defence and Marine,Energy,Manufacturing, including Industrial Biotechology,Transport
Impact Types Societal,Economic

 
Description SAE AMS-AM (Aerospace Materials Specification - Additive Manufacturing) Standard committee
Geographic Reach Multiple continents/international 
Policy Influence Type Participation in a guidance/advisory committee
Impact The AMS-AM standards will promote the adoption of environmental friendly additive manufacturing technology in aerospace and wider industrial sectors worldwide.
URL http://profiles.sae.org/teaamsam-m/
 
Description Collaboration with Airbus 
Organisation Airbus Group
Department Airbus Operations
Country United Kingdom 
Sector Private 
PI Contribution Developed and supplied "low alloy steel powder" to Airbus to develop alternative manufacturing process for large aircraft components. Further two stainless grades (13-8Mo, 15-5PH) have been developed and supplied to a new collaboration project "I-Break" led by Airbus. Liberty Powder Metals hasn't been included as a formal partner in the I-Break project due to funding restriction on Liberty. However, conversion with Airbus is on-going and Airbus is planning to ask the business to join the project once the ownership of the business is changed therefore funding restriction is removed.
Collaborator Contribution Airbus are coordinating with partners to assess the alternative manufacturing processes. Based on the initial findings Airbus has initiated a large collaboration project "I-Break" partial funded by ATI in 2022. Currently the I-Break project is evaluating new manufacturing processes using powders developed by Liberty.
Impact A large collaboration project "Landing Gear Industrial Breakthroughs (I-Break)" led by Airbus has been funded by ATI. This project will shape Airbus Landing Systems, its ecosystem of partners and suppliers.
Start Year 2021
 
Description Collaboration with Prof. Pedro Rivera at University of Lancaster 
Organisation Lancaster University
Department Department of Engineering
Country United Kingdom 
Sector Academic/University 
PI Contribution Prof. Pedro Rivera is Liberty / Royal Academy of Engineering Research Chair at University of Lancaster. The collaboration with Prof. Pedro has centred on novel powder alloy development for additive manufacturing. Our team has provided market insight and technical guidance on alloy design and produced modified alloy powder for further study by Prof. Pedro's team. Standard alloy powder has also been provided for comparison. Results fro printing trial and mechanical testing of 17-4PH+ powder are very promising. Liberty is in preparation to apply a new patent together with Prof. Pedro Rivera. Additional17-4PH+ powder has been produced for further testing. Three new grades of tool steel AM powders have been developed and supplied to partner.
Collaborator Contribution Alloy design calculations, microstructure analysis and mechanical testing of additive manufactured standard and new alloys.
Impact Prof. Pedro has been invited to give a keynote lecture at MSE-Congress2022, Germany, talking about the latest results of this collaboration. A new patent application is currently in preparation.
Start Year 2021
 
Title A METHOD OF METAL ADDITIVE MANUFACTURING 
Description A method of manufacturing an article by metal additive manufacture (MAM), the method comprises: providing a steel-based atomised powder composition comprising manganese and sulphur, wherein the sulphur content is in the range of 0.01 to 0.1 wt.% of the total composition, and the weight percentage ratio of Mn:S is greater than or equal to 5, preferably greater than or equal to 10; providing a layer of the atomised powder composition; melting and cooling the layer. repeating to form an article, wherein the article comprises nanosized MnS particles. There is also disclosed a metal additive manufactured article formed of steel having small grain size. 
IP Reference WO2021079133 
Protection Patent application published
Year Protection Granted 2021
Licensed Commercial In Confidence
Impact It is expected this patent will lead to revenue at Liberty Powder Metals in the value of £3m in the next five years from sale of invented alloy powder.
 
Title Powder production process improvement 
Description Powder production process has been improved through process innovation, in the area of slag control, refractory material selection and process optimisation. 
Type Of Technology New/Improved Technique/Technology 
Year Produced 2021 
Impact In the past year, productivity improved by over 50% and out-of-spec product rate reduced by over 30% at Liberty Powder Metals. Enabled 5 new powder grades produced. 
 
Description Co-supervise EngD student at Sheffield University 
Form Of Engagement Activity A formal working group, expert panel or dialogue
Part Of Official Scheme? No
Geographic Reach Local
Primary Audience Postgraduate students
Results and Impact Liberty Powder Metals Limited and Johnson Matthey Limited are the industrial sponsor of EngD student Natasha Eades at the Department of Metallurgy and Materials, University of Sheffield. Natasha works on a project titled "Powder Metallurgical Approaches to Graded Alloy Microstructures for Enhanced Surface Properties". Our team provided metal powder, application knowledge and technical guidance to Natash through quarterly meeting and email communications.


Brief description of the research project:
The understanding of microstructures and their effect upon alloy properties is an integral part of metallurgical processing. Enhancement of alloy performance has been achieved for ranges of alloys by addition of minor elements and thermomechanical processing, thereby manipulating the chemistries and microstructures to provide desired benefits. However, such additions and processing steps are generally performed on bulk alloys, often resulting in undesirable costs in finished components arising from the presence of expensive elemental additions in areas where they serve no purpose. Such issues can be circumvented, for example, by deposition of surface coatings. However, thin surface coatings can be subject to degradation by in-use environmental conditions, exposing the underlying unprotected alloy and shortening component lifetime.

In this project we will examine routes for generating asymmetric "graded" alloy microstructures to provide property enhancement at the surface of components, where they are needed, avoiding the cost of bulk alloying additions. Concentrating upon powder metallurgical processing to generate the graded microstructures, we will examine the introduction of precious metals into steels and nickel superalloys, examining the effect upon the microstructures, the interactions of the modified microstructures with the underlying base alloys, thermomechanical properties and corrosion resistance under environmental conditions relevant to the end-use applications of those alloys. The industrial partners, Johnson Matthey and Liberty Powder Metals, will work closely with the student to provide complementary manufacturing and characterization facilities to enrich the project investigations.
Year(s) Of Engagement Activity 2021,2022,2023
 
Description Co-supervise PhD student at Nottingham University 
Form Of Engagement Activity A formal working group, expert panel or dialogue
Part Of Official Scheme? No
Geographic Reach Local
Primary Audience Postgraduate students
Results and Impact Liberty Powder Metals Limited is the industrial sponsor of PhD student Ian Marsh at Faculty of Engineering, University of Nottingham. Ian works on a research project "High Integrity Additive Manufacturing Using Recovered Material Feedstocks". Our team has provided metal powders, application knowledge and technical guidance to Ian. We have also hosted Ian at our site for a week for Ian to learn powder production process, powder characterisation techniques and operation process of a new additive manufacture machine.
Ian has continued his work last year. However, recently he decided to change his PhD to Master degree and pursue a career in industry.
Year(s) Of Engagement Activity 2021,2022