High Resolution Silicon Strip Detectors for portable mass spectrometry

Lead Research Organisation: University of Liverpool
Department Name: Physics

Abstract

We will develop a mass spectrometer based on high resolution micro-strip silicon detectors as a sensing element. This novel approach intends to significant improve the mass resolution and sensitivity with respect to current technology. It aims to separate the different ions of the injected cold gas with an electric and magnetic field and subsequently accelerate the ions to sufficient energy to release detectable signal in the micro-strip detector. The instrument is comprised of a source of the cold gas to be analysed (sample), two evacuated drift sections and the sensing device. A state of the art cold ion source to feed in the proposed instrument will be built and provided by the project partner Q-T. The first drift section is about 5-10 cm long, with a low tuneable electric field (up to 10 V/cm) and a magnetic field to allow for separation of the ions with different mass during their drift toward the acceleration section. This acceleration section (with a length of 15-20 cm and an electric field of 500-1500 V/cm) allows impacting the ions onto the sensing element with sufficient energy to record the signal that determines the hit unambiguous position. The sensing element is a silicon micro-strip detector with 128 readout channel with a resolution of less than 10 micrometers. The clock rate of the electronics is 40MHz (or the integration time is 25 ns) and the total readout time for the sensor is 3.2 microseconds. The electric field in the mass separation section is tuned to optimise the mass separation in the region of interest. Scanning this electric field allows for studying a wide range of masses with this compact instrument.

Planned Impact

The improvement of the performance of portable mass spectrometers leads to major advantages for deploying the instrument in locations such as border security checkpoints at airports etc to complement the work of sniffer dogs. Outside the area of security, such an instrument could have further impact on medical diagnostics (e.g.through patient breath analysis and /or analysis of bodily fluids via paperspray sample injection).

The beneficiary of this research will be society at large, through the improved security yielded by more sensitive, portable instruments apt to detect explosive, human presence and/or drugs at border or police checkpoints; through the availability of portable and fast diagnostic tools for a range of diseases. Industry can benefit from affordable instruments for analyzing waste and oil-in-water contents.

The prototype/demonstrator equipment object of the research here proposed will pave the way for instruments that can become available to users within a couple of year time.

Publications

10 25 50
 
Description Data recently taken have proven the concept and now encourage seeking for IP. The feasibility of high mass resolution portable spectrometers is an attractive feature for many applications (security, portable analysis...). The tests have indicated that further improvements are possible and technical changes with impact in this field of technology and science are envisaged.
Exploitation Route With refinement of the sensors used, for higher spatial resolution and mainly lower noise performance for reduction of the required high electrical drifting field, further improvement in sensitivity and portability can be achieved that were not envisageable before these tests.
Sectors Aerospace, Defence and Marine,Culture, Heritage, Museums and Collections,Security and Diplomacy

 
Description The results have been presented to a few commercial company with interests in security and open possible commercial channels. This though requires further refinement of the system developed. We have tested the prorotype and now seeking for application possibilities.
First Year Of Impact 2015
Sector Aerospace, Defence and Marine,Electronics
Impact Types Cultural,Societal

 
Title Improvement of sensitivity for spectroscopy instruments 
Description Change in approach to high sensitivity spectroscopy. 
Type Of Material Improvements to research infrastructure 
Provided To Others? No  
Impact The application of the research results is in progress. 
 
Description Q Technologies 
Organisation Q Technologies Ltd
Country United Kingdom 
Sector Private 
PI Contribution Deep knowledge of the snsing elements (silicon detrectors). New ideas for a novel approach to spectrometry. Realisation of the concept.
Collaborator Contribution Expertise and in kind of controlled ion source. Expertise in commercial, portable spectrometers.
Impact The results of this collaboration could be taken into the commercial products of the company.
Start Year 2015