A Study of Friction in Composite Materials Forming

Lead Research Organisation: University of Glasgow
Department Name: School of Engineering

Abstract

The composite materials industry is rapidly growing in response to the need to conserve energy and reduce emissions by reducing weight - particularly in transport sectors such as automotive and aerospace. Many composite parts are produced using a forming process (especially those with irregular shapes). In such processes, it is essential that the final component meets the design specifications and is free from wrinkles, voids and unwanted thickness variations. At present, however, the only way to ensure success is to carry out costly trial and error type testing in advance. Since the component geometries can change on a regular basis, the forming industry would like to have a predictive tool which can predict outcomes and can therefore be used to set up the process optimally to produce the required part. A crucial job of any predictive model is to predict the forming forces. One of the important forces acting during the forming process is friction. To correctly predict friction forces in forming, an underlying physical understanding of the frictional behaviour must be developed and the frictional response using relevant fabric and resin types must be characterised. Some friction tests have been carried out previously, but these have often been idealised or on small contact areas which are not representative. This project will design experiments to give representative friction force measurements for different fabric and resin systems under a wide range of boundary conditions. A database of results will be established giving the friction response to changes in the various variables affecting friction such as resin type, fabric type, temperature, normal load and shear rate etc. Both tool-ply and ply-ply friction will be investigated. An ABAQUS user subroutine based on the experimental database will then be developed to model the contact behaviour. This predictive capability for friction in the forming process will then be added to presently available forming models within our group to improve their forming predictions. Finally, the model will be validated by comparing predictions with test results for some case-study type forming examples. The project will produce a valuable physical description of friction in forming, a database of relevant results and a predictive subroutine which can be added to existing models to increase their accuracy. The result will be a significant step in the direction of accurate predictive forming models which have the potential to reduce costs considerably and to optimise products. A final aspect of the project will be to look at viable approaches to reducing friction during the forming process.

Publications

10 25 50
 
Description Investigation was carried out into the use of interlayers to reduce friction between composite plys in high temperature press forming

Composite materials consist of a (usually) polymer matrix reinforced by a woven fiber sheets(glass fiber, carbon fiber etc). When press formed into complex shapes these woven fiber sheets must be able to slide and rotate relative to each other. If they cannot do this then there is a tendency wrinkles to appear in the final part. These wrinkles reduce the strength of the final part.

The ability for these to slide and rotate is governed by the frictional forces between two sheets. Normally this is carried out in a molten polymer (eg nylon) which has a high viscosity much like honey and limits the ability to slide and rotate. The use of a low viscosity inter layer was proposed to lower friction and allow for more complex shapes to be formed. In this investigation Carbon Fiber Reinforced Nylon has been paired with interlayers of tin due to their similar melt points (~230 Celcius). Use of a metallic interlayer also led to other novel points which are discussed below

(1) Induction Heating-
-Press forming conventionally uses radiant heaters and a shuttle system to heat and move the sheets into place.
- The use of a metallic interlayer allows for heat to be generated directly into the sample allowing for in situ heating (no shuttle) and reduced temperature requirements of the surrounding apparatus
- Equipment was rented and due to time limitations we were not able to fully optimise the heating process which limited control over forming temperature. Trial and error and user expertise was used and a "feedback loop" involving infrared cameras was set up

(2) Multi step press forming tool
- This was driven by a desire to remove tin interlayer from final part during forming
- A multi step tool of interlocking concentric tubes was used to form from the center out
- Forming from the center out produced a pressure gradient which removed the tin
- Multi stage forming also allows for improved forming of multi cavity parts which can be an issue in single step forming.

(3) Results of the experiments
- We were able to produce a number of succesful samples (both flat and with a multi cavity ripple shape). However we have not had enough time with the testing apparatus to identify best practices
- To date we have quantified the levels of residual tin which can be brought down to ~2-5% of part volume. This was quantified using a combination of Computed Tomography Scans, Conventional X rays and microscope analysis of polished cross sections.
- We have not yet confirmed the effects of the residual tin on the mechanical properties, however mechanical testing will soon be carried out in order to quantify this.
- We have not carried out a comparison with samples containing no interlayer. This is also planned for future works.
Exploitation Route Academically the department is applying for a core project through the EPSRC Future Composites Manufacturing Research Hub with the following objectives
1. Take methods to improve the process (develop control system to manage heating of larger parts, analysis of parameters such as speed of press forming, pressure applied, thickness of interlayer, temperature of forming)
2. Extend the investigation to other material combinations
3. Extend investigation into the multi step forming tool

In industry

This is a much more long term project which deliberately attempting a step change. Long term, if proven effective, this could be used in composites manufacturing which is rapidly expanding. Potential benefits include
Increased energy efficiency through being able to heat the sample directly and without shuttling the sample.
Ability to form more complex shapes with less wrinkling or other defects
Sectors Aerospace, Defence and Marine,Manufacturing, including Industrial Biotechology