University of Nottingham - Equipment Account
Lead Research Organisation:
University of Nottingham
Department Name: Research and Innovation (Admin)
Abstract
Summary
We will offer to UK academic and industrial scientists and engineers expert facilitated access to a new high performance liquids dedicated XPS spectrometer, the first of its kind in the UK. This type of instrument is an important tool used across many science and engineering disciplines, including for example nanotechnology, chemistry, surface science, functional materials, pharmaceuticals, catalysis, metallurgy, sensors, the environment and energy. LiPPS will provide unique atomistic measurements of both bulk liquids and solutes there-in. Other new features make this instrument easier to operate, able to deal with a wider range of sample types and to acquire data autonomously.
This unique facility will provide UK universities and industry with the opportunity to carry out world-leading research. By providing open access at the Nottingham Nanotechnology and Nanoscience Centre (NNNC) at the University of Nottingham we aim to maximise the impact of this instrument on UK science and industry. To help achieve this Nottingham will collaborate with other leading centres of Photoelectron Electron Spectroscopy particularly the new national facility (NEXUS) hosted by Newcastle.
The NNNC operates as a sustainable cross-faculty multidisciplinary centre supporting open-access to state-of the art-instrumentation. The provision of such facilities is a priority of the University of Nottingham. The new LiPPS instrument will become a key service within the NNNC which is committed to the long term maintenance and updating of this resource for the benefit of research in the UK.
We will offer to UK academic and industrial scientists and engineers expert facilitated access to a new high performance liquids dedicated XPS spectrometer, the first of its kind in the UK. This type of instrument is an important tool used across many science and engineering disciplines, including for example nanotechnology, chemistry, surface science, functional materials, pharmaceuticals, catalysis, metallurgy, sensors, the environment and energy. LiPPS will provide unique atomistic measurements of both bulk liquids and solutes there-in. Other new features make this instrument easier to operate, able to deal with a wider range of sample types and to acquire data autonomously.
This unique facility will provide UK universities and industry with the opportunity to carry out world-leading research. By providing open access at the Nottingham Nanotechnology and Nanoscience Centre (NNNC) at the University of Nottingham we aim to maximise the impact of this instrument on UK science and industry. To help achieve this Nottingham will collaborate with other leading centres of Photoelectron Electron Spectroscopy particularly the new national facility (NEXUS) hosted by Newcastle.
The NNNC operates as a sustainable cross-faculty multidisciplinary centre supporting open-access to state-of the art-instrumentation. The provision of such facilities is a priority of the University of Nottingham. The new LiPPS instrument will become a key service within the NNNC which is committed to the long term maintenance and updating of this resource for the benefit of research in the UK.
Planned Impact
Impact Summary
Who will benefit?
The proposal will help support and generate research projects that drive new areas of activity across UK HEIs. These are expected to be primarily within the areas of (or at the interface of) catalysis, nanotechnology, chemistry, surface science, functional materials, pharmaceuticals, biotechnology, food technology, the environment and energy. Resulting outputs will potentially benefit the wider scientific community and UK industry, increasing international competiveness.
The project will benefit the Universities in this proposal through increased integration of facilitated open access to liquid based XPS. This initial collaboration on offering complementary EPSRC National Facility (NEXUS) services hosted by the University of Newcastle. The University of Nottingham will benefit through experience gained in the sustainable operation of an open access analytical facility working in partnership, as opposed to competitively, with other HEIs. The NNNC will also benefit through the increased number of users within the Centre that may also access other complementary tools.
New fundamental insights and applications delivered through the analysis supplied will benefit academics through generating new avenues for research. The LiPPS instrument will provide proof of principle data and detailed study data that users can obtain to leverage higher quality research outputs and financial support. We foresee that benefits will also accrue to the applicants and associated research groups in Physics, Pharmacy and Chemistry in terms of collaborations spinning out from the activities of the Centre. Such collaborations may also occur between users of the Centre, either through direct linking through the Centre itself or at user meetings. Industrial users will benefit from access to state of the art analyses and expertise which can much more rapidly address problems than current systems. As well as increased sample throughput the system will provide a range of quantitative data that can help inform business critical decisions.
How will benefit from the research be supported?
As specified in our proposal, time on instrumentation or training will be allocated based upon a hierarchical question system. This will lead to the selection of Users with interests in line with EPSRC remit and work with maximum benefit to the user and the UK. Academic and industrial researchers will be trained as required in new analytical and data interpretation skills. Hence the LiPPS will contribute to delivering a source of highly trained researchers with significant added skills.
As appropriate we will facilitate technology transfer through engagement with regional and national networks (eg. KTNs) through the BDE within the NNNC, the Universities Research and Business Development Office and its wholly owned TSB funded technology transfer company, eminate Ltd. Whilst XPS is an established technique in certain high-value industrial sectors (eg. semiconductors, aerospace, pharmaceuticals), this completely new approach of liquid XPS measurements will lead to a step-change in the application of XPS to analytical measurements.
Training benefits (eg. improved career prospects) and the impact of industrial problem solving are expected to accrue from 6 months. Research outputs such as publications, talks at conferences and funding are expected to begin from around 12-18 months of project commencement. A contribution to new substantive collaborations that yield significant areas of activity and identifiable industrial outputs such as products/IP will be from years 2 to 3.
Who will benefit?
The proposal will help support and generate research projects that drive new areas of activity across UK HEIs. These are expected to be primarily within the areas of (or at the interface of) catalysis, nanotechnology, chemistry, surface science, functional materials, pharmaceuticals, biotechnology, food technology, the environment and energy. Resulting outputs will potentially benefit the wider scientific community and UK industry, increasing international competiveness.
The project will benefit the Universities in this proposal through increased integration of facilitated open access to liquid based XPS. This initial collaboration on offering complementary EPSRC National Facility (NEXUS) services hosted by the University of Newcastle. The University of Nottingham will benefit through experience gained in the sustainable operation of an open access analytical facility working in partnership, as opposed to competitively, with other HEIs. The NNNC will also benefit through the increased number of users within the Centre that may also access other complementary tools.
New fundamental insights and applications delivered through the analysis supplied will benefit academics through generating new avenues for research. The LiPPS instrument will provide proof of principle data and detailed study data that users can obtain to leverage higher quality research outputs and financial support. We foresee that benefits will also accrue to the applicants and associated research groups in Physics, Pharmacy and Chemistry in terms of collaborations spinning out from the activities of the Centre. Such collaborations may also occur between users of the Centre, either through direct linking through the Centre itself or at user meetings. Industrial users will benefit from access to state of the art analyses and expertise which can much more rapidly address problems than current systems. As well as increased sample throughput the system will provide a range of quantitative data that can help inform business critical decisions.
How will benefit from the research be supported?
As specified in our proposal, time on instrumentation or training will be allocated based upon a hierarchical question system. This will lead to the selection of Users with interests in line with EPSRC remit and work with maximum benefit to the user and the UK. Academic and industrial researchers will be trained as required in new analytical and data interpretation skills. Hence the LiPPS will contribute to delivering a source of highly trained researchers with significant added skills.
As appropriate we will facilitate technology transfer through engagement with regional and national networks (eg. KTNs) through the BDE within the NNNC, the Universities Research and Business Development Office and its wholly owned TSB funded technology transfer company, eminate Ltd. Whilst XPS is an established technique in certain high-value industrial sectors (eg. semiconductors, aerospace, pharmaceuticals), this completely new approach of liquid XPS measurements will lead to a step-change in the application of XPS to analytical measurements.
Training benefits (eg. improved career prospects) and the impact of industrial problem solving are expected to accrue from 6 months. Research outputs such as publications, talks at conferences and funding are expected to begin from around 12-18 months of project commencement. A contribution to new substantive collaborations that yield significant areas of activity and identifiable industrial outputs such as products/IP will be from years 2 to 3.
Publications
Adam M
(2018)
Microwave synthesis of carbon onions in fractal aggregates using heavy oil as a precursor
in Carbon
Agyakwa P
(2016)
Damage Evolution in Al Wire Bonds Subjected to a Junction Temperature Fluctuation of 30 K
in Journal of Electronic Materials
Albar JD
(2017)
An atomic carbon source for high temperature molecular beam epitaxy of graphene.
in Scientific reports
Alenezi T
(2019)
A novel type cold mix pavement material made with calcium-alginate and aggregates
in Journal of Cleaner Production
Algodi S
(2018)
Wear performance of TiC/Fe cermet electrical discharge coatings
in Wear
Alvarez-Paino M
(2019)
Polymer Microparticles with Defined Surface Chemistry and Topography Mediate the Formation of Stem Cell Aggregates and Cardiomyocyte Function.
in ACS applied materials & interfaces
Arjmand E
(2016)
Predicting Lifetime of Thick Al Wire Bonds Using Signals Obtained From Ultrasonic Generator
in IEEE Transactions on Components, Packaging and Manufacturing Technology
Arjmand E
(2016)
A thermal cycling reliability study of ultrasonically bonded copper wires
in Microelectronics Reliability
Astle M
(2019)
Molybdenum Dioxide in Carbon Nanoreactors as a Catalytic Nanosponge for the Efficient Desulfurization of Liquid Fuels
in Advanced Functional Materials
Title | Art installation at the nmRC |
Description | An art competition was held within the Nanoscale and Microscale Research Centre (nmRC), targeting staff and students who utilise our EPSRC instrumentation. We received over 30 entries, with winning entries curated into an exhibition wall within the nmRC. |
Type Of Art | Artistic/Creative Exhibition |
Year Produced | 2023 |
Impact | Launch of the public outreach programme (Under the Microscope). Positive feedback from visitors on the creativity of the centre. |
URL | https://www.nottingham.ac.uk/nmrc/under-the-microscope.aspx |
Description | Axis Ultra DLD LiPPS: Development of new depth/layering models for ionic solutions in their solid, liquid and a glass states. Tof SIMS gas cluster ion beam: This system has allowed studies of polymer multi-layer systems in collaboration with NPL. Results will be used to guide users in the optimisation of their instrument use. Research relating to the depth profiling of organic materials, such as demonstrating variations in polymer structures used in animal surgeries, are now also possible. Instrument: nanobeam nb5: Developed method to transfer metallic patterns to the end of optical fibres, with the results presented at international conference (photics west 22). |
Exploitation Route | Axis Ultra DLD LiPPS: In the near future the XPS is expected the be used to characterize subtle fluorine chemistry changes nanobeam nb5 Products in development with Cancer Research UK to be used for the detection of cancer cells. Quanta 650 ESEM This instrument is used frequently to image biomedical implants and biomaterials for slow release drug development. It has also been used to look at implants removed from patients, and some in-vivo implants in mice. |
Sectors | Chemicals Pharmaceuticals and Medical Biotechnology |
URL | http://www.nottingham.ac.uk/nnnc/index.aspx |
Description | This award supports a range of instruments, and there have been a number of non academic impacts as summarised below: Instrument: Quanta650 ESEM - This instrument is used frequently to image biomedical implants and biomaterials for slow release drug development. It has also been used to look at implants removed from patients, and some in-vivo implants in mice. alongside this, a commissioned artist used images from this instrument to produce art work now displayed in the Carbon Neutral Lab (CNL), Jubilee Campus, University of Nottingham. Instrument: nanobeam nb5 - Products in development with Cancer Research UK to be used for the detection of cancer cells. |
First Year Of Impact | 2021 |
Sector | Creative Economy,Pharmaceuticals and Medical Biotechnology |
Impact Types | Cultural Societal Policy & public services |
Description | A New Correlative Approach for Structure Determination & Imaging of Molecular Materials |
Amount | £1,470,902 (GBP) |
Funding ID | EP/W006413/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 12/2021 |
End | 11/2026 |
Description | AWE Research Funding |
Amount | £616,848 (GBP) |
Funding ID | PO 30351471/26 |
Organisation | Atomic Weapons Establishment |
Sector | Private |
Country | United Kingdom |
Start | 06/2015 |
End | 12/2018 |
Description | An integrated assessment of UK Shale resource distribution based on fundamental analyses of shale mechanical & fluid properties. |
Amount | £254,307 (GBP) |
Funding ID | NE/R018030/1 |
Organisation | Natural Environment Research Council |
Sector | Public |
Country | United Kingdom |
Start | 08/2018 |
End | 08/2022 |
Description | BBSRC Training Grant |
Amount | £95,042 (GBP) |
Funding ID | BB/N503617/1 |
Organisation | Biotechnology and Biological Sciences Research Council (BBSRC) |
Sector | Public |
Country | United Kingdom |
Start | 06/2016 |
End | 06/2020 |
Description | EMPIR |
Amount | € 1,798,279 (EUR) |
Funding ID | 17IND08 (AdvanCT) |
Organisation | European Commission |
Department | Horizon 2020 |
Sector | Public |
Country | European Union (EU) |
Start | 05/2018 |
End | 05/2021 |
Description | EMPIR |
Amount | € 2,000,000 (EUR) |
Funding ID | 15HLT01 |
Organisation | European Commission |
Department | Horizon 2020 |
Sector | Public |
Country | European Union (EU) |
Start | 03/2016 |
End | 03/2020 |
Description | EPSRC Programme Grant |
Amount | £6,331,952 (GBP) |
Funding ID | EP/N035437/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 06/2016 |
End | 07/2021 |
Description | EPSRC Research Grant |
Amount | £910,916 (GBP) |
Funding ID | EP/P019080/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 02/2017 |
End | 01/2020 |
Description | EPSRC Research Grant |
Amount | £481,397 (GBP) |
Funding ID | EP/L013908/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 05/2014 |
End | 05/2017 |
Description | EPSRC Research Grant |
Amount | £736,411 (GBP) |
Funding ID | EP/N03404X/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 08/2016 |
End | 08/2019 |
Description | EPSRC Standard Research |
Amount | £783,422 (GBP) |
Funding ID | EP/N033906/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 09/2016 |
End | 09/2019 |
Description | EPSRC Strategic Equipment |
Amount | £2,019,330 (GBP) |
Funding ID | EP/P029868/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 07/2017 |
End | 07/2022 |
Description | EPSRC award |
Amount | £3,531,769 (GBP) |
Funding ID | EP/N024818/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 09/2016 |
End | 09/2020 |
Description | Growth of hexagonal boron nitride for deep ultraviolet photonics, quantum emitters and van der Waals substrates |
Amount | £1,027,022 (GBP) |
Funding ID | EP/V05323X/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 11/2021 |
End | 07/2024 |
Description | High resolution, cryogenic analytical and transfer scanning electron microscope (HR-CAT-SEM) |
Amount | £1,564,542 (GBP) |
Funding ID | EP/S021434/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 03/2019 |
End | 03/2025 |
Description | KTP Partnership |
Amount | £150,000 (GBP) |
Funding ID | 510929 |
Organisation | Innovate UK |
Sector | Public |
Country | United Kingdom |
Start | 04/2016 |
End | 04/2019 |
Description | Leverhulme Trust Research Grant RPG-2014-129 "Molecular Beam Epitaxy for Graphene/Boron Nitride electronics" |
Amount | £132,073 (GBP) |
Organisation | The Leverhulme Trust |
Sector | Charity/Non Profit |
Country | United Kingdom |
Start | 02/2015 |
End | 02/2018 |
Description | Lewerhulme Trust Research Grant |
Amount | £132,073 (GBP) |
Funding ID | RPG-2014-129 |
Organisation | The Leverhulme Trust |
Sector | Charity/Non Profit |
Country | United Kingdom |
Start | 02/2015 |
End | 03/2018 |
Description | Maximising existing equipment |
Amount | £202,437 (GBP) |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 03/2018 |
End | 03/2020 |
Description | Meta-fibres: Optical fibres with meta-surfaces for advanced optical biopsy through needles |
Amount | £1,222,168 (GBP) |
Funding ID | MR/T041951/1 |
Organisation | Medical Research Council (MRC) |
Sector | Public |
Country | United Kingdom |
Start | 01/2021 |
End | 12/2024 |
Description | Metal Atoms on Surfaces & Interfaces (MASI) for Sustainable Future |
Amount | £6,659,514 (GBP) |
Funding ID | EP/V000055/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 07/2021 |
End | 07/2026 |
Description | NanoPrime: Maximising Equipment and Expertise Sharing in Nanoscience |
Amount | £202,437 (GBP) |
Funding ID | EP/R025282/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 03/2018 |
End | 03/2022 |
Description | Nanoscale Characterisation of Biological and Bioinspired Materials using Integrated Fluidic Force - High-Resolution Confocal Microscopy |
Amount | £777,905 (GBP) |
Funding ID | BB/W019639/1 |
Organisation | Biotechnology and Biological Sciences Research Council (BBSRC) |
Sector | Public |
Country | United Kingdom |
Start | 07/2022 |
End | 07/2023 |
Description | Programme Grant |
Amount | £5,365,958 (GBP) |
Funding ID | EP/N006615/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 11/2015 |
End | 11/2020 |
Description | Programme Grant |
Amount | £6,486,390 (GBP) |
Funding ID | EP/P013341/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 02/2017 |
End | 02/2022 |
Description | Programme Grants |
Amount | £5,365,958 (GBP) |
Funding ID | EP/N006615/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 11/2015 |
End | 11/2020 |
Description | Seed Award |
Amount | £250,000 (GBP) |
Funding ID | 201457/Z/16/Z |
Organisation | Wellcome Trust |
Sector | Charity/Non Profit |
Country | United Kingdom |
Start | 03/2017 |
End | 03/2021 |
Description | Strain-engineered graphene: growth, modification and electronic properties |
Amount | £910,916 (GBP) |
Funding ID | EP/P019080/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 02/2017 |
End | 01/2021 |
Title | Cryogenic FIB lift-out |
Description | The preparation of thinned lamellae from bulk samples for transmission electron microscopy (TEM) analysis has been possible in the focussed ion beam scanning electron microscope (FIB-SEM) for over 20 years via the in situ lift-out method. Lift-out offers a fast and site specific preparation method for TEM analysis, typically in the field of materials science. More recently it has been applied to a low-water content biological sample (Rubino 2012). This work presents the successful lift-out of high-water content lamellae, under cryogenic conditions (cryo-FIB lift-out) and using a nanomanipulator retaining its full range of motion, which are advances on the work previously done by Rubino (2012). Strategies are explored for maintaining cryogenic conditions, grid attachment using cryo-condensation of water and protection of the lamella when transferring to the TEM |
Type Of Material | Improvements to research infrastructure |
Year Produced | 2016 |
Provided To Others? | Yes |
Impact | Two citations Crygenic FIBSEM workshop 2017 to be held at the nmRC. These skills will be demonstrated to a group of industrial and academic experts in this research field. |
URL | https://www.scopus.com/record/display.uri?eid=2-s2.0-84975725988&doi=10.1002%2fjemt.22630&origin=inw... |
Title | DNP assisted ssNMR |
Description | Enhancement of solid state NMR using the polarization arising from unpaired electrons. The polarization is transferred by means of a strong microwave field under cryogenic conditions. |
Type Of Material | Improvements to research infrastructure |
Year Produced | 2016 |
Provided To Others? | Yes |
Impact | Provision of this research tool fills a gap in the UK NMR instrumentation landscape, identified in a survey carried out 2013 and listed as priority in the UK NMR roadmap 2014. |
URL | http://www.notttingham.ac.uk/dnpnmr |
Title | CCDC 1811026: Experimental Crystal Structure Determination |
Description | Related Article: Mary Robert Garrett, María Jesús Durán-Peña, William Lewis, Kaspars Pudzs, Janis Užulis, Igors Mihailovs, Björk Tyril, Jonathan Shine, Emily F. Smith, Martins Rutkis, Simon Woodward|2018|J.Mater.Chem.C|6|3403|doi:10.1039/C8TC00073E |
Type Of Material | Database/Collection of data |
Year Produced | 2018 |
Provided To Others? | Yes |
URL | http://www.ccdc.cam.ac.uk/services/structure_request?id=doi:10.5517/ccdc.csd.cc1ysj6g&sid=DataCite |
Title | CCDC 2004404: Experimental Crystal Structure Determination |
Description | Related Article: Toby J. Blundell, Laurence J. Taylor, Andrew J. Valentine, William Lewis, Alexander J. Blake, Jonathan McMaster, Deborah L. Kays|2020|Chem.Commun.|56|8139|doi:10.1039/D0CC03559A |
Type Of Material | Database/Collection of data |
Year Produced | 2020 |
Provided To Others? | Yes |
URL | http://www.ccdc.cam.ac.uk/services/structure_request?id=doi:10.5517/ccdc.csd.cc258r6f&sid=DataCite |
Title | CCDC 2004405: Experimental Crystal Structure Determination |
Description | Related Article: Toby J. Blundell, Laurence J. Taylor, Andrew J. Valentine, William Lewis, Alexander J. Blake, Jonathan McMaster, Deborah L. Kays|2020|Chem.Commun.|56|8139|doi:10.1039/D0CC03559A |
Type Of Material | Database/Collection of data |
Year Produced | 2020 |
Provided To Others? | Yes |
URL | http://www.ccdc.cam.ac.uk/services/structure_request?id=doi:10.5517/ccdc.csd.cc258r7g&sid=DataCite |
Title | CCDC 2004406: Experimental Crystal Structure Determination |
Description | Related Article: Toby J. Blundell, Laurence J. Taylor, Andrew J. Valentine, William Lewis, Alexander J. Blake, Jonathan McMaster, Deborah L. Kays|2020|Chem.Commun.|56|8139|doi:10.1039/D0CC03559A |
Type Of Material | Database/Collection of data |
Year Produced | 2020 |
Provided To Others? | Yes |
URL | http://www.ccdc.cam.ac.uk/services/structure_request?id=doi:10.5517/ccdc.csd.cc258r8h&sid=DataCite |
Title | CCDC 2004407: Experimental Crystal Structure Determination |
Description | Related Article: Toby J. Blundell, Laurence J. Taylor, Andrew J. Valentine, William Lewis, Alexander J. Blake, Jonathan McMaster, Deborah L. Kays|2020|Chem.Commun.|56|8139|doi:10.1039/D0CC03559A |
Type Of Material | Database/Collection of data |
Year Produced | 2020 |
Provided To Others? | Yes |
URL | http://www.ccdc.cam.ac.uk/services/structure_request?id=doi:10.5517/ccdc.csd.cc258r9j&sid=DataCite |
Title | CCDC 2004408: Experimental Crystal Structure Determination |
Description | Related Article: Toby J. Blundell, Laurence J. Taylor, Andrew J. Valentine, William Lewis, Alexander J. Blake, Jonathan McMaster, Deborah L. Kays|2020|Chem.Commun.|56|8139|doi:10.1039/D0CC03559A |
Type Of Material | Database/Collection of data |
Year Produced | 2020 |
Provided To Others? | Yes |
URL | http://www.ccdc.cam.ac.uk/services/structure_request?id=doi:10.5517/ccdc.csd.cc258rbk&sid=DataCite |
Title | CCDC 2045511: Experimental Crystal Structure Determination |
Description | Related Article: Coby J. Clarke, Patrick J. Morgan, Jason P. Hallett, Peter Licence|2021|ACS Sustain.Chem.Eng.|9|6224|doi:10.1021/acssuschemeng.0c08564 |
Type Of Material | Database/Collection of data |
Year Produced | 2021 |
Provided To Others? | Yes |
URL | http://www.ccdc.cam.ac.uk/services/structure_request?id=doi:10.5517/ccdc.csd.cc26nj7n&sid=DataCite |
Title | CCDC 2045512: Experimental Crystal Structure Determination |
Description | Related Article: Coby J. Clarke, Patrick J. Morgan, Jason P. Hallett, Peter Licence|2021|ACS Sustain.Chem.Eng.|9|6224|doi:10.1021/acssuschemeng.0c08564 |
Type Of Material | Database/Collection of data |
Year Produced | 2021 |
Provided To Others? | Yes |
URL | http://www.ccdc.cam.ac.uk/services/structure_request?id=doi:10.5517/ccdc.csd.cc26nj8p&sid=DataCite |
Title | CCDC 2045513: Experimental Crystal Structure Determination |
Description | Related Article: Coby J. Clarke, Patrick J. Morgan, Jason P. Hallett, Peter Licence|2021|ACS Sustain.Chem.Eng.|9|6224|doi:10.1021/acssuschemeng.0c08564 |
Type Of Material | Database/Collection of data |
Year Produced | 2021 |
Provided To Others? | Yes |
URL | http://www.ccdc.cam.ac.uk/services/structure_request?id=doi:10.5517/ccdc.csd.cc26nj9q&sid=DataCite |
Description | CT-STARR (CT-Surface Texture for Additive Round Robin) |
Organisation | National Physical Laboratory |
Country | United Kingdom |
Sector | Academic/University |
PI Contribution | Conducted round robin comparative measurement of a Ti6Al4V ELI sample |
Collaborator Contribution | Conducted round robin comparative measurement of a Ti6Al4V ELI sample |
Impact | The comparative study validates the parameter extraction process, provides useful repeatability and reproducibility data and provides baseline information for an expanded, Stage 2, round robin. |
Start Year | 2016 |
Description | CT-STARR (CT-Surface Texture for Additive Round Robin) |
Organisation | University of Huddersfield |
Country | United Kingdom |
Sector | Academic/University |
PI Contribution | Conducted round robin comparative measurement of a Ti6Al4V ELI sample |
Collaborator Contribution | Conducted round robin comparative measurement of a Ti6Al4V ELI sample |
Impact | The comparative study validates the parameter extraction process, provides useful repeatability and reproducibility data and provides baseline information for an expanded, Stage 2, round robin. |
Start Year | 2016 |
Description | CT-STARR (CT-Surface Texture for Additive Round Robin) |
Organisation | X-Tek Systems Ltd (Nikon Metrology UK Ltd) |
Country | United Kingdom |
Sector | Private |
PI Contribution | Conducted round robin comparative measurement of a Ti6Al4V ELI sample |
Collaborator Contribution | Conducted round robin comparative measurement of a Ti6Al4V ELI sample |
Impact | The comparative study validates the parameter extraction process, provides useful repeatability and reproducibility data and provides baseline information for an expanded, Stage 2, round robin. |
Start Year | 2016 |
Description | Identification of carbenium ions in zeolite and their interaction with the surface probed by DNP enhanced solid-state NMR |
Organisation | University of Liverpool |
Department | Department of Cellular and Molecular Physiology |
Country | United Kingdom |
Sector | Academic/University |
PI Contribution | The research team helped in setting up the experiments and aided in sample preparation. The research team also provided scientific inputs as and when applicable. |
Collaborator Contribution | The contribution helped in investigation of zeolitic materials using dynamic nuclear polarization (DNP) assisted magic-angle spinning(MAS) assisted solid-state Nuclear Magnetic Resonance (ssNMR). The collaborating partners primarily carried out the experiments in our facility. They brought the samples to be investigated. |
Impact | We have initially performed 13C and 29Si DNP MAS NMR at 14.09 T on a range of zeolites with various physical properties, including a range of particle size and pore structures. The results obtained will be used further in the investigation of zeolites using DNP. The collaboration is multi-disciplinary. It involves the discipline of physics and chemistry. |
Start Year | 2015 |
Description | Investigation of dangling bonds assisted polarization enhancement for pure silicon nanoparticles |
Organisation | Dartmouth College |
Department | Department of Physics and Astronomy |
Country | United States |
Sector | Academic/University |
PI Contribution | The research team from University of Nottingham provided scientific inputs, ideas and expertise to help exploring this first of its kind study of utilizing intrinsic biradicals for DNP in MAS NMR. The research team also helped in setting up of experiments and preparation of samples. |
Collaborator Contribution | The partner contributed in exchange of expertise and scientific ideas. PhD students from the collaborators group came to Nottingham to carry out experiments. They also carried out low temperature EPR studies in their lab which helped us in understanding the nature of these biradicals. |
Impact | Initially we used the dangling bonds on the surface of these materials to enhance the NMR signals. It was seen for the first time that such methods can be exploited in MAS DNP studies. Further studies were carried out using exogenous radicals which proved to be more efficient in this case, but also showed us that if the dangling bonds concentration can be increased, then exogenous radical scenario can be emulated. The collaboration is multi-disciplinary. It involves the discipline of physics, chemistry, and nanoscience. |
Start Year | 2016 |
Description | CMG annual meeting |
Form Of Engagement Activity | A formal working group, expert panel or dialogue |
Part Of Official Scheme? | No |
Geographic Reach | National |
Primary Audience | Professional Practitioners |
Results and Impact | Cryo Microscopy Group annual meeting |
Year(s) Of Engagement Activity | 2018 |
URL | http://www.cryomicroscopygroup.org.uk/CMG2018.php |
Description | CMG meeting |
Form Of Engagement Activity | Participation in an activity, workshop or similar |
Part Of Official Scheme? | No |
Geographic Reach | National |
Primary Audience | Professional Practitioners |
Results and Impact | The nmRC hosted the 2016 CryoMicroscopy Group meeting with 60+ delegates. This event included presentations by invited speakers, posters, exhibitor stands and also a workshop (for those interested in cryogenic transfer techniques). |
Year(s) Of Engagement Activity | 2016 |
URL | http://www.cryomicroscopygroup.org.uk/CMG2016.php |
Description | DNP Converence |
Form Of Engagement Activity | A talk or presentation |
Part Of Official Scheme? | No |
Geographic Reach | National |
Primary Audience | Postgraduate students |
Results and Impact | The intended purpose was to make the studies done in our facility known to a broader audience, and entice more researchers/industry personnel towards this relatively new scientific technique. |
Year(s) Of Engagement Activity | 2016 |
Description | DNP Launch Event |
Form Of Engagement Activity | Participation in an activity, workshop or similar |
Part Of Official Scheme? | No |
Geographic Reach | International |
Primary Audience | Professional Practitioners |
Results and Impact | The intended purpose was to make the studies done in our facility known to a broader audience, and entice more researchers/industry personnel towards this relatively new scientific technique. |
Year(s) Of Engagement Activity | 2015 |
Description | FutForm training workshop |
Form Of Engagement Activity | Participation in an activity, workshop or similar |
Part Of Official Scheme? | No |
Geographic Reach | International |
Primary Audience | Postgraduate students |
Results and Impact | Graham Rance, Michael Fay, Chris Parmenter, Emily Smith FutForm Annual Meeting and Training Workshop, University of Nottingham, Nottingham, UK, 6th June 2017, oral presentations. FutForm is a H2020 RISE project on 'Future Formulations: Developing Future Pharmaceuticals Through Advanced Analysis and Intersectoral Exchange' with participants from Portugal, Netherlands and Italy. |
Year(s) Of Engagement Activity | 2017 |
URL | http://www.cordis.europa.eu/project/rcn/199941_en.html |
Description | NUAST |
Form Of Engagement Activity | Participation in an open day or visit at my research institution |
Part Of Official Scheme? | No |
Geographic Reach | Local |
Primary Audience | Schools |
Results and Impact | Graham Rance, Michael Fay, Christine Grainger-Boultby Nottingham University Academy of Science and Technology (NUAST), 14th July 2016 and 13th July 2017. |
Year(s) Of Engagement Activity | 2017 |
Description | Prof Novikov's video press release |
Form Of Engagement Activity | A press release, press conference or response to a media enquiry/interview |
Part Of Official Scheme? | No |
Geographic Reach | International |
Primary Audience | Media (as a channel to the public) |
Results and Impact | Prof Novikov's video press release, prepared by Nottingham press office for the Opening Day of the graphene MBE facilities on the 08.01.2015 (https://mediaspace.nottingham.ac.uk/media/Growing+graphene+%E2%80%93+blue+sky+research+attempts+to+replicate+nature/1_rwzc7u6k/ or on YouTube https://www.youtube.com/watch?v=A6obEfjWj3Y |
Year(s) Of Engagement Activity | 2015 |
URL | https://www.youtube.com/watch?v=A6obEfjWj3Y |
Description | Queen's birthday |
Form Of Engagement Activity | A broadcast e.g. TV/radio/film/podcast (other than news/press) |
Part Of Official Scheme? | No |
Geographic Reach | International |
Primary Audience | Public/other audiences |
Results and Impact | The nmRC used a FIBSEM to etch a birthday message to the Queen for her 90th birthday (which coincided with the opening of the centre). The FIBSEM etching and imaging was recorded and shown on the BBC news; described on a BBC world service radio interview and was picked up by other news outlets and social media. The etched corgi hair is now kept at Windsor Castle in a glass corgi for posterity. |
Year(s) Of Engagement Activity | 2016 |
URL | http://www.bbc.co.uk/news/uk-england-nottinghamshire-36099200 |
Description | Saharan dust |
Form Of Engagement Activity | A press release, press conference or response to a media enquiry/interview |
Part Of Official Scheme? | No |
Geographic Reach | National |
Primary Audience | Media (as a channel to the public) |
Results and Impact | Dr Beth Steer collected dust particles (from Saharan red sky in October) from her car windscreen to take a look at them under a scanning electron microscope (SEM). Story tweeted by the Nanoscale and Microscale Research Centre (nmRC) and was picked up by BBC national news. |
Year(s) Of Engagement Activity | 2017 |
URL | https://www.nottingham.ac.uk/nmrc/news/nmrc-sem-images-of-saharan-dust-on-bbc-news.aspx |
Description | School involvement/widening participation (Nottingham) |
Form Of Engagement Activity | Participation in an open day or visit at my research institution |
Part Of Official Scheme? | No |
Geographic Reach | Local |
Primary Audience | Schools |
Results and Impact | Year 12 STEM students from NUAST were given an introduction to SEM and TEM techniques. |
Year(s) Of Engagement Activity | 2018 |
Description | Soot Workshop |
Form Of Engagement Activity | Participation in an activity, workshop or similar |
Part Of Official Scheme? | No |
Geographic Reach | National |
Primary Audience | Postgraduate students |
Results and Impact | Graham Rance, Michael Fay, Chris Parmenter EPSRC Soot: Nanoparticle Characterisation and Morphology Workshop, University of Nottingham, Nottingham, UK, 29th March 2017, oral and poster presentations. |
Year(s) Of Engagement Activity | 2017 |
URL | https://www.nottingham.ac.uk/nmrc/news/soot-in-oil-diagnostics.aspx |
Description | Under the microscope |
Form Of Engagement Activity | Engagement focused website, blog or social media channel |
Part Of Official Scheme? | No |
Geographic Reach | National |
Primary Audience | Public/other audiences |
Results and Impact | An outreach activity called 'under the microscope' has been advertised online and via social media channels from the Nanoscale and Microscale Research Centre. This utilises EPSRC funded instrumentation to take a closer look at samples provided by the general public. This has been picked up by local news coverage and will advertised on TV and radio from 13th March 2023. |
Year(s) Of Engagement Activity | 2023 |
URL | https://www.nottingham.ac.uk/nmrc/under-the-microscope.aspx |
Description | World's smallest periodic table created at the University of Nottingham, press release |
Form Of Engagement Activity | A press release, press conference or response to a media enquiry/interview |
Part Of Official Scheme? | No |
Geographic Reach | National |
Primary Audience | Public/other audiences |
Results and Impact | In honour of his visit on the 13th March the team in the nmRC have achieved a new record for the smallest periodic table alongside a miniaturised portrait of Oganessian and the creator of the periodic table Dmitri Mendeleev. Professor Yuri Oganessian is the only living person to have an element in the Periodic Table named after him and is giving a special lecture at the University as part of their celebrations to mark the 150th anniversary of the Periodic Table. The final design of this special periodic table gift measures just 14 x 7 µm which is over 6 times smaller than the previous record and the largest dimension is smaller than the diameter of a single fibre of merino wool. The individual lines in the letters are around 30 nm which is about the size of the smallest virus. The portraits' thickness range from 100 nm to 1 µm meaning they are about 1000 times thinner than a single layer of skin. Dr Richard Cousins is an electron beam lithography technician and created the piece. Electron beam lithography (EBL) uses a beam of high energy electrons to define a pattern on a thin polymer film, referred to as a resist. The beam of electrons which has a diameter of just a few nanometres (nm) is precisely directed onto the resist-coated silicon chip. When the beam hits the chip it interacts with the resist causing its properties to change. Development of the resist then transfers the pattern onto the silicon chip, which was then further processed to create either the portrait or the periodic table. Media piece written about is research (URL listed below) which has been picked up by various media outlets such as Chemistry World. We have plans to develop this further in the future. |
Year(s) Of Engagement Activity | 2019 |
URL | https://www.nottingham.ac.uk/news/pressreleases/2019/mar/yuri-periodic-table.aspx |
Description | XEN Workshop, Natural History Museum, London |
Form Of Engagement Activity | Participation in an activity, workshop or similar |
Part Of Official Scheme? | No |
Geographic Reach | International |
Primary Audience | Industry/Business |
Results and Impact | Conference |
Year(s) Of Engagement Activity | 2017 |
Description | Xradia European Network (XEN) meeting |
Form Of Engagement Activity | Participation in an activity, workshop or similar |
Part Of Official Scheme? | No |
Geographic Reach | International |
Primary Audience | Industry/Business |
Results and Impact | Conference |
Year(s) Of Engagement Activity | 2015 |
Description | nmRC School Visit (NUAST) |
Form Of Engagement Activity | Participation in an open day or visit at my research institution |
Part Of Official Scheme? | No |
Geographic Reach | Local |
Primary Audience | Schools |
Results and Impact | students from a local high school (NUAST) visited the nmRC facility. Students were given a tour of the centre and were shown how to operate and image using SEM and TEM. |
Year(s) Of Engagement Activity | 2016 |
Description | nmRC Twitter Feed |
Form Of Engagement Activity | Engagement focused website, blog or social media channel |
Part Of Official Scheme? | No |
Geographic Reach | International |
Primary Audience | Public/other audiences |
Results and Impact | The Nanoscale and Microscale Research Centre (nmRC) started a twitter feed in September 2017. There are now approximately 100 followers including a BBC News Reader and also Professor Sir Fraser Stoddart (winner of 2016 Nobel Prize in chemistry). We have had success with the BBC picking up two news stories through this feed. We also use the feed to advertise PhD studentships and other noteworthy related items. |
Year(s) Of Engagement Activity | 2017 |
URL | https://twitter.com/uonnmrc |