Micro Materials NanoTest Vantage Testing Suite with NTX4Controller
Lead Research Organisation:
University of Southampton
Department Name: Faculty of Engineering & the Environment
Abstract
The proposed bid will provide the UK with a world leading nanomechanical and nanotribological testing facility, with access available to all UK academic institutions and UK industry. The Micro Materials Vantage System represents a step-change in repositioning accuracy and testing speed than previous systems. It provides the ability to undertake 6 fundamentally different mechanical or tribological tests (Indentation, Scratch, Impact, Fatigue, Wear, Fretting), in a range of different environments, offering the ability to tailor tests to simulate service environments.
The ability to mechanically and tribologically test at the nano-scale is vitally important for a number of different scientific disciplines.
In Tribology, the behaviour of macro-scale contacts such as the bearing surface contact of a hip joint, is governed by the interfacial interactions at the nano-scale. Assessment of the nanomechanical and nanotribological behaviour of the surfaces, and the investigation of the surface layers or tribofilms formed during contact motion, is vital to the fundamental understanding of the contacts behaviour, and it provides crucial information for predictive modelling.
In manufacturing and materials science, new manufacturing and processing techniques such as laser processing and electrical discharge machining, produce microstructures, thin surface layers and textures on material surfaces which are of the order of microns in size. This means conventional hardness, wear and impact testing methods are simply not sufficient to assess them. This microstructure and texture formation can enhance and detract from the performance of the component in service; therefore the ability to test relevant properties at the appropriate scale is vital.
Coatings science is a field which spans a multitude of disciplines ranging from ship antifouling paint films through to hard coatings for the turbine blades of jet engines. While these coatings can vary in thickness, hard coatings for wear, impact and erosion resistance can be typically 1-50 microns thick with properties tailored to fit their purpose. The low thicknesses of the coatings mean their adhesion to the substrate and mechanical properties which are vital to the prediction of their performance can only be accessed through nano-scale testing.
Many natural materials such as bone and cartilage have complex hierarchical structures which extending down to the nano-scale. Changes occurring at the nano and micro-scale govern the macro-scale properties and performance and the ability to assess these levels provides valuable insights into the origins of conditions such as Osteoarthritis and Osteoporosis.
The ability to mechanically and tribologically test at the nano-scale is vitally important for a number of different scientific disciplines.
In Tribology, the behaviour of macro-scale contacts such as the bearing surface contact of a hip joint, is governed by the interfacial interactions at the nano-scale. Assessment of the nanomechanical and nanotribological behaviour of the surfaces, and the investigation of the surface layers or tribofilms formed during contact motion, is vital to the fundamental understanding of the contacts behaviour, and it provides crucial information for predictive modelling.
In manufacturing and materials science, new manufacturing and processing techniques such as laser processing and electrical discharge machining, produce microstructures, thin surface layers and textures on material surfaces which are of the order of microns in size. This means conventional hardness, wear and impact testing methods are simply not sufficient to assess them. This microstructure and texture formation can enhance and detract from the performance of the component in service; therefore the ability to test relevant properties at the appropriate scale is vital.
Coatings science is a field which spans a multitude of disciplines ranging from ship antifouling paint films through to hard coatings for the turbine blades of jet engines. While these coatings can vary in thickness, hard coatings for wear, impact and erosion resistance can be typically 1-50 microns thick with properties tailored to fit their purpose. The low thicknesses of the coatings mean their adhesion to the substrate and mechanical properties which are vital to the prediction of their performance can only be accessed through nano-scale testing.
Many natural materials such as bone and cartilage have complex hierarchical structures which extending down to the nano-scale. Changes occurring at the nano and micro-scale govern the macro-scale properties and performance and the ability to assess these levels provides valuable insights into the origins of conditions such as Osteoarthritis and Osteoporosis.
Planned Impact
This system will impact on a number of important areas including Society, Knowledge, the Economy and People.
Knowledge: The Vantage system already represents a step-change in nanomechanical and nanotribological testing. The unique range of tests, the environments under which they can be performed, the positioning, load and displacement accuracy, all mean that this system will open novel areas of research, whilst remaining at the forefront of the testing world for the foreseeable future. The historical links between Micro Materials Ltd. and nCATS provides a platform for new technique development, as will the new interactions between Micro Materials Ltd. and innovative researchers from the user group. The system will help to forge new collaborations and skill sharing between The University of Southampton, The University of Sheffield, The University of Nottingham and The University of Portsmouth.
People: The EPSRC Review of Mechanical Engineering 2011 noted: 'Serious concerns about the difficulty that exists in recruiting and retaining UK trained doctoral students'. Access to cutting edge equipment and infrastructure has a huge impact on an institutions ability to attract and retain top quality researchers. While this equipment would directly benefit four UK universities, it will allow access to other new users, supporting UK science as a whole. The system would be based at the University of Southampton within the national Centre for Advanced Tribology at Southampton (nCATS). The centre was established as a response to the recognition that despite Tribology's importance to the UK economy and to UK industry, it was a declining discipline. Globally it is recognised that 1-3% of GDP loss is attributable to friction and wear, which in the UK represents ~£65 Billion. The Vantage system would further reinvigorate an important field of research and assist with the attraction of new people to the field.
Economic and Societal Impact: MML are a UK company producing a world leading piece of equipment. The purchase of the Vantage system would represent a significant investment and boost to a UK company. The equipment's positioning at Southampton and usage by other UK Universities and industry will generate high quality research outputs. These outputs will be seen globally, helping to boost the profile of the user's research but strengthen MML's position as a provider of world leading equipment. The advances in the speed of testing offered by this system means that series of tests can be performed in a fraction of that time previously required, enhancing the overall output of the system but also allowing for a major cost saving for users as they will be required to pay for less time on the system.
Outreach to new users: Time will be allocated for use of the system by individuals outside of the main users identified in this proposal. All the user groups have extensive links with industry and collaborations with other universities. nCATS alone has 30 industrial partners and a total of ~100 companies with whom it directly interacts. These companies would be made directly aware of the new system and its capabilities. nCATS has an active outreach programme to the UK academic and industrial community in place and frequently hosts events such as EWTEC 2011, (European Wave and Tidal Energy Conference, 5-9 September 2011) and the Materials KTN and nCATS 'Functional Coatings - A Workshop on Coatings beyond REACh' (February 22nd 2012 - about 80 participants from 50 companies). Future events would showcase and advertise the systems capabilities, attracting new users to the system. In addition nCATS has a strong history of outreach outside of industry and academia, evidenced recently by the UK Tribology Network (UKTN) event held at Southampton (05/03/2012), where the public were invited to introductory talks about Tribology by Professor Robert Wood (Director of nCATS and chair of the UK Tribology Network).
Knowledge: The Vantage system already represents a step-change in nanomechanical and nanotribological testing. The unique range of tests, the environments under which they can be performed, the positioning, load and displacement accuracy, all mean that this system will open novel areas of research, whilst remaining at the forefront of the testing world for the foreseeable future. The historical links between Micro Materials Ltd. and nCATS provides a platform for new technique development, as will the new interactions between Micro Materials Ltd. and innovative researchers from the user group. The system will help to forge new collaborations and skill sharing between The University of Southampton, The University of Sheffield, The University of Nottingham and The University of Portsmouth.
People: The EPSRC Review of Mechanical Engineering 2011 noted: 'Serious concerns about the difficulty that exists in recruiting and retaining UK trained doctoral students'. Access to cutting edge equipment and infrastructure has a huge impact on an institutions ability to attract and retain top quality researchers. While this equipment would directly benefit four UK universities, it will allow access to other new users, supporting UK science as a whole. The system would be based at the University of Southampton within the national Centre for Advanced Tribology at Southampton (nCATS). The centre was established as a response to the recognition that despite Tribology's importance to the UK economy and to UK industry, it was a declining discipline. Globally it is recognised that 1-3% of GDP loss is attributable to friction and wear, which in the UK represents ~£65 Billion. The Vantage system would further reinvigorate an important field of research and assist with the attraction of new people to the field.
Economic and Societal Impact: MML are a UK company producing a world leading piece of equipment. The purchase of the Vantage system would represent a significant investment and boost to a UK company. The equipment's positioning at Southampton and usage by other UK Universities and industry will generate high quality research outputs. These outputs will be seen globally, helping to boost the profile of the user's research but strengthen MML's position as a provider of world leading equipment. The advances in the speed of testing offered by this system means that series of tests can be performed in a fraction of that time previously required, enhancing the overall output of the system but also allowing for a major cost saving for users as they will be required to pay for less time on the system.
Outreach to new users: Time will be allocated for use of the system by individuals outside of the main users identified in this proposal. All the user groups have extensive links with industry and collaborations with other universities. nCATS alone has 30 industrial partners and a total of ~100 companies with whom it directly interacts. These companies would be made directly aware of the new system and its capabilities. nCATS has an active outreach programme to the UK academic and industrial community in place and frequently hosts events such as EWTEC 2011, (European Wave and Tidal Energy Conference, 5-9 September 2011) and the Materials KTN and nCATS 'Functional Coatings - A Workshop on Coatings beyond REACh' (February 22nd 2012 - about 80 participants from 50 companies). Future events would showcase and advertise the systems capabilities, attracting new users to the system. In addition nCATS has a strong history of outreach outside of industry and academia, evidenced recently by the UK Tribology Network (UKTN) event held at Southampton (05/03/2012), where the public were invited to introductory talks about Tribology by Professor Robert Wood (Director of nCATS and chair of the UK Tribology Network).
Publications
Alshammary B
(2016)
The importance of the film structure during self-powered ibuprofen salicylate drug release from polypyrrole electrodeposited on AZ31 Mg
in Journal of Solid State Electrochemistry
Bahrami A
(2019)
Mechanical properties and microstructural stability of CuTa/Cu composite coatings
in Surface and Coatings Technology
Callisti M
(2015)
Ni-Ti(-Cu) shape memory alloy interlayers supporting low friction functional coatings
in Tribology International
Callisti M
(2016)
Bubbles formation in helium ion irradiated Cu/W multilayer nanocomposites: Effects on structure and mechanical properties
in Journal of Nuclear Materials
Callisti M
(2014)
The role of Ni-Ti-(Cu) interlayers on the mechanical properties and nano-scratch behaviour of solid lubricant W-S-C coatings
in Surface and Coatings Technology
Callisti M
(2014)
Microstructural investigation on the grain refinement occurring in Cu-doped Ni-Ti thin films
in Scripta Materialia
Callisti M
(2016)
Structural and mechanical properties of ?-irradiated Zr/Nb multilayer nanocomposites
in Materials Letters
Callisti M
(2017)
Combined size and texture-dependent deformation and strengthening mechanisms in Zr/Nb nano-multilayers
in Acta Materialia
Callisti M
(2015)
Microstructural evolution of nanometric Ti(NiCu)2 precipitates in annealed Ni-Ti-Cu thin films
in Vacuum
Callisti M
(2015)
Stress-induced martensitic transformation in Ni-Ti(-Cu) interlayers controlling stress distribution in functional coatings during sliding
in Applied Surface Science
Callisti M
(2018)
Competing mechanisms on the strength of ion-irradiated Zr/Nb nanoscale multilayers: Interface strength versus radiation hardening
in Scripta Materialia
Cifuentes S
(2017)
Assessment of mechanical behavior of PLA composites reinforced with Mg micro-particles through depth-sensing indentations analysis
in Journal of the Mechanical Behavior of Biomedical Materials
Escudeiro A
(2015)
Structural and mechanical properties of nanocrystalline Zr co-sputtered a-C(:H) amorphous films
in Applied Surface Science
Evaristo M
(2014)
Tribological behaviour of W-alloyed carbon-based coatings in dry and lubricated sliding contact TRIBOLOGICAL BEHAVIOUR OF W-ALLOYED CARBON-BASED COATINGS
in Lubrication Science
Fernandes F
(2015)
Tribological properties of self-lubricating TiSiVN coatings at room temperature
in Surface and Coatings Technology
Fernandes F
(2014)
The effect of increasing V content on the structure, mechanical properties and oxidation resistance of Ti-Si-V-N films deposited by DC reactive magnetron sputtering
in Applied Surface Science
Fernandes F
(2018)
Tribological and cutting performance of TiAlCrN films with different Cr contents deposited with multilayered structure
in Tribology International
Frutos E
(2019)
The role of a? orthorhombic phase content on the tenacity and fracture toughness behavior of Ti-22Nb-10Zr coating used in the design of long-term medical implants
in Applied Surface Science
Frutos E
(2016)
Repetitive nano-impact tests as a new tool to measure fracture toughness in brittle materials
in Journal of the European Ceramic Society
Frutos E
(2021)
Effect of substrate bias voltage on the mechanical properties and deformation mechanisms in the nanostructured Ti-22Nb-10Zr coating
in Surface and Coatings Technology
Frutos E
(2015)
Length-scale-dependent mechanical behaviour of Zr/Nb multilayers as a function of individual layer thickness
in Materials Science and Engineering: A
Frutos E
(2016)
Nanomechanical characterization of alumina coatings grown on FeCrAl alloy by thermal oxidation.
in Journal of the mechanical behavior of biomedical materials
Frutos E
(2018)
Development of new ß/a?-Ti-Nb-Zr biocompatible coating with low Young's modulus and high toughness for medical applications
in Materials & Design
Hudec T
(2019)
Structure, mechanical and tribological properties of Mo-S-N solid lubricant coatings
in Applied Surface Science
Jonnalagadda US
(2018)
Acoustically modulated biomechanical stimulation for human cartilage tissue engineering.
in Lab on a chip
Description | This project covered the management costs of strategic funding by EPSRC. The funded device allows analysis of mechanical properties at nanonoscale, such as hardness and elastic modulus, in different conditions (temperature, impact, etc). So far we published over30 papers using the equipment and established new research lines in material science and biomechanics. The equipment was essential to win significant grant portfolio, such as H2020 FET Open project, H2020 MSCA project (we are coordinators), EPSRC Prosperous NaTion project, two Newton Advanced Fellowships and many more. |
Exploitation Route | We explore the full potential of the device and prepare a new method on how to evaluate nanomechanical data. Our processes are shared through scientific publications. |
Sectors | Aerospace Defence and Marine Manufacturing including Industrial Biotechology |
Description | We have a number of consultancy work using the device from leading aerospace companies and the health sector. Total income was over 100k. |
First Year Of Impact | 2013 |
Sector | Aerospace, Defence and Marine,Healthcare,Manufacturing, including Industrial Biotechology |
Impact Types | Economic |
Description | (MDOT) - Medical Device Obligations Taskforce |
Amount | € 8,944,243 (EUR) |
Funding ID | 814654 |
Organisation | European Commission |
Sector | Public |
Country | European Union (EU) |
Start | 01/2019 |
End | 12/2023 |
Description | HardAlt: New generation of protective coatings alternative to hard chrome |
Amount | € 395,000 (EUR) |
Funding ID | 606110 |
Organisation | European Commission |
Department | Seventh Framework Programme (FP7) |
Sector | Public |
Country | European Union (EU) |
Start | 12/2013 |
End | 11/2016 |
Description | Renaissance of alloys: nanocrystalline bimetals |
Amount | £223,099 (GBP) |
Funding ID | EP/R041768/1 |
Organisation | Engineering and Physical Sciences Research Council (EPSRC) |
Sector | Public |
Country | United Kingdom |
Start | 03/2018 |
End | 03/2020 |
Description | Solution |
Amount | € 3,504,101 (EUR) |
Organisation | European Commission H2020 |
Sector | Public |
Country | Belgium |
Start | 02/2017 |
End | 01/2021 |
Description | Solid lubricant coatings |
Organisation | Czech Technical University in Prague |
Country | Czech Republic |
Sector | Academic/University |
PI Contribution | We provide nanoscale analysis of solid lubricant coatings produces in Prague or Coimbra (part of EU project we coordinate). |
Collaborator Contribution | Our partners fabricate coatings tested in Southampton. |
Impact | Several papers (attached). |
Start Year | 2013 |
Description | Solid lubricant coatings |
Organisation | University of Coimbra |
Country | Portugal |
Sector | Academic/University |
PI Contribution | We provide nanoscale analysis of solid lubricant coatings produces in Prague or Coimbra (part of EU project we coordinate). |
Collaborator Contribution | Our partners fabricate coatings tested in Southampton. |
Impact | Several papers (attached). |
Start Year | 2013 |